Dibenzofuran-3-yl(phenyl)methanone

Base Information

• Chemical Name: Dibenzofuran-3-yl(phenyl)methanone
• CAS No.: 6407-29-0
• Molecular Formula: C19H12 O2
• Molecular Weight: 272.303
• European Community (EC) Number: 660-876-0
• DSSTox Substance ID: DTXSID50274734
• Wikidata: Q82004173
• Mol file: 6407-29-0.mol

Synonyms:dibenzofuran-3-yl(phenyl)methanone;6407-29-0;3-benzoyldibenzofuran;DTXSID50274734;AKOS025128049;dibenzo[b,d]furan-3-yl(phenyl)methanone

Chemical Property of Dibenzofuran-3-yl(phenyl)methanone

Chemical Property:

• Vapor Pressure: 3.57E-08mmHg at 25°C
• Refractive Index: 1.5510 (estimate)
• Boiling Point: 446.7°Cat760mmHg
• Flash Point: 217.6°C
• PSA: 30.21000
• Density: 1.245g/cm³
• LogP: 4.81700
• XLogP3: 5.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 272.083729621
• Heavy Atom Count: 21
• Complexity: 385

Purity/Quality:

2-Benzoyldibenzofuran ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)C2=CC3=C(C=C2)C4=CC=CC=C4O3

Technology Process of Dibenzofuran-3-yl(phenyl)methanone

There total 8 articles about Dibenzofuran-3-yl(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

dibenzofuran (132-64-9,214827-48-2) + benzoyl chloride (98-88-4) → 1-(dibenzo[b,d]furan-2-yl)(phenyl)methanone (6407-29-0)

Guidance literature:

With aluminum (III) chloride; at 20 ℃; for 8h;

DOI:10.1021/jacs.7b08710

Reference yield: 13.0%

p-phenoxybenzophenone (6317-73-3) → 1-(dibenzo[b,d]furan-2-yl)(phenyl)methanone (6407-29-0) + 11H-Fluoreno<3,2-b>benzofuran-11-on (121073-95-8)

Guidance literature:

With palladium diacetate; In acetic acid; for 24h; Heating;

Reference yield:

N,N-dimethyldibenzo[b,d]furan-2-carboxamide + phenyllithium (591-51-5) → 1-(dibenzo[b,d]furan-2-yl)(phenyl)methanone (6407-29-0)

Guidance literature:

phenyllithium; With n-butyllithium; In tetrahydrofuran; dibutyl ether; at -78 ℃; for 0.5h; Inert atmosphere;

N,N-dimethyldibenzo[b,d]furan-2-carboxamide; In tetrahydrofuran; dibutyl ether; at -78 - 0 ℃; Inert atmosphere;

upstream raw materials:

dibenzofuran

benzoyl chloride

benzoic acid anhydride

p-phenoxybenzophenone

Downstream raw materials:

2-Benzyl-dibenzofuran

1-(dibenzo[b,d]furan-2-yl(phenyl)methyl)-2-methyl-1H-imidazole

1-(dibenzo[b,d]furan-2-yl(phenyl)methyl)-1H-benzo[d]imidazole

1-(dibenzo[b,d]furan-2-yl(phenyl)methyl)-3-butyl-1H-imidazol-3-ium iodide