4-NITROPHENOXYACETIC ACID HYDRAZIDE

Base Information

• Chemical Name: 4-NITROPHENOXYACETIC ACID HYDRAZIDE
• CAS No.: 75129-74-7
• Molecular Formula: C8H9N3O4
• Molecular Weight: 211.177
• Hs Code.: 2928000090
• Mol file: 75129-74-7.mol

Synonyms:Aceticacid, (4-nitrophenoxy)-, hydrazide (9CI);Acetic acid, (p-nitrophenoxy)-,hydrazide (6CI,7CI);(4-Nitrophenoxy)acetic acid hydrazide;2-(4-Nitrophenoxy)acetic hydrazide;2-(4-Nitrophenoxy)acetohydrazide;NSC77505;p-Nitrophenoxyacetohydrazide;p-Nitrophenoxyacetyl hydrazide;

Chemical Property of 4-NITROPHENOXYACETIC ACID HYDRAZIDE

Chemical Property:

• Vapor Pressure: 1.35E-10mmHg at 25°C
• Melting Point: 184-186°C
• Refractive Index: 1.592
• Boiling Point: 511.9 °C at 760 mmHg
• Flash Point: 263.4 °C
• PSA: 110.17000
• Density: 1.394 g/cm³
• LogP: 1.57790

Purity/Quality:

97% ^*data from raw suppliers

4-NitrophenoxyaceticAcidHydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-NITROPHENOXYACETIC ACID HYDRAZIDE

There total 8 articles about 4-NITROPHENOXYACETIC ACID HYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methyl 2-(4-nitrophenoxy)acetate (19786-48-2) → (4-nitro-phenoxy)-acetic acid hydrazide (75129-74-7)

Guidance literature:

With hydrazine hydrate; In methanol; for 0.0166667h; microwave irradiation;

DOI:10.1081/SCC-120027275

Reference yield: 85.0%

ethyl 4-nitrophenoxyacetate (19076-89-2) → (4-nitro-phenoxy)-acetic acid hydrazide (75129-74-7)

Guidance literature:

With hydrazine hydrate; In ethanol; Reflux;

DOI:10.2174/1570180813666160805150148

Reference yield: 24.0%

C13H15NO7 → (4-nitro-phenoxy)-acetic acid hydrazide (75129-74-7)

Guidance literature:

With hydrazine; In tetrahydrofuran; at 0 ℃; for 2h;

upstream raw materials:

ethyl 4-nitrophenoxyacetate

4-nitrophenoxyacetic acid

methyl 2-(4-nitrophenoxy)acetate

4-nitro-phenol

Downstream raw materials:

5-(4-nitro-phenoxymethyl)-[1,3,4]oxadiazol-2-ylamine

(4-Nitro-phenoxy)-acetic acid [5-methyl-2-oxo-1,2-dihydro-indol-(3Z)-ylidene]-hydrazide

C₂₄H₂₁N₇O₄

C₂₅H₂₃N₇O₄