Technology Process of Benzene,
1-(1,5-dimethyl-4-hexenyl)-2,5-bis(methoxymethoxy)-4-methyl-
There total 23 articles about Benzene,
1-(1,5-dimethyl-4-hexenyl)-2,5-bis(methoxymethoxy)-4-methyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-bromo-6-methylhept-5-ene;
With
zinc;
In
tetrahydrofuran;
2,5-bis(methoxymethoxy)-4-bromotoluene;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
tetrahydrofuran;
for 24h;
Heating;
DOI:10.1021/jo035778s
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 68 percent / BF3*Et2O / -78 °C
2: H2 / 20percent Pd(OH)2/C
3: pyridine
4: 73 percent / NaBH4 / dimethylsulfoxide
5: 96 percent / pyridine
6: AlCl3 / C2H5SH
7: NaH, 18-crown-6 / acetonitrile
8: 88 percent / 2N aq. NaOH / methanol
9: PCC / CH2Cl2
10: NaH / dimethylsulfoxide
With
pyridine; sodium hydroxide; sodium tetrahydroborate; aluminium trichloride; 18-crown-6 ether; boron trifluoride diethyl etherate; hydrogen; sodium hydride; pyridinium chlorochromate;
palladium dihydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; acetonitrile; ethanethiol;
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 68 percent / BF3*Et2O / -78 °C
2: H2 / 20percent Pd(OH)2/C
3: pyridine
4: 73 percent / NaBH4 / dimethylsulfoxide
5: 96 percent / pyridine
6: AlCl3 / C2H5SH
7: NaH, 18-crown-6 / acetonitrile
8: 88 percent / 2N aq. NaOH / methanol
9: PCC / CH2Cl2
10: NaH / dimethylsulfoxide
With
pyridine; sodium hydroxide; sodium tetrahydroborate; aluminium trichloride; 18-crown-6 ether; boron trifluoride diethyl etherate; hydrogen; sodium hydride; pyridinium chlorochromate;
palladium dihydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; acetonitrile; ethanethiol;