Technology Process of 4-(2,5-Bis-methoxymethoxy-4-methyl-phenyl)-pentanal
There total 19 articles about 4-(2,5-Bis-methoxymethoxy-4-methyl-phenyl)-pentanal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 68 percent / BF3*Et2O / -78 °C
2: H2 / 20percent Pd(OH)2/C
3: pyridine
4: 73 percent / NaBH4 / dimethylsulfoxide
5: 96 percent / pyridine
6: AlCl3 / C2H5SH
7: NaH, 18-crown-6 / acetonitrile
8: 88 percent / 2N aq. NaOH / methanol
9: PCC / CH2Cl2
With
pyridine; sodium hydroxide; sodium tetrahydroborate; aluminium trichloride; 18-crown-6 ether; boron trifluoride diethyl etherate; hydrogen; sodium hydride; pyridinium chlorochromate;
palladium dihydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; acetonitrile; ethanethiol;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 68 percent / BF3*Et2O / -78 °C
2: H2 / 20percent Pd(OH)2/C
3: pyridine
4: 73 percent / NaBH4 / dimethylsulfoxide
5: 96 percent / pyridine
6: AlCl3 / C2H5SH
7: NaH, 18-crown-6 / acetonitrile
8: 88 percent / 2N aq. NaOH / methanol
9: PCC / CH2Cl2
With
pyridine; sodium hydroxide; sodium tetrahydroborate; aluminium trichloride; 18-crown-6 ether; boron trifluoride diethyl etherate; hydrogen; sodium hydride; pyridinium chlorochromate;
palladium dihydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; acetonitrile; ethanethiol;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: H2 / 20percent Pd(OH)2/C
2: pyridine
3: 73 percent / NaBH4 / dimethylsulfoxide
4: 96 percent / pyridine
5: AlCl3 / C2H5SH
6: NaH, 18-crown-6 / acetonitrile
7: 88 percent / 2N aq. NaOH / methanol
8: PCC / CH2Cl2
With
pyridine; sodium hydroxide; sodium tetrahydroborate; aluminium trichloride; 18-crown-6 ether; hydrogen; sodium hydride; pyridinium chlorochromate;
palladium dihydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; acetonitrile; ethanethiol;