Benzene,1-(1,2-diphenyl-1-buten-1-yl)-4-methoxy-

Base Information

• Chemical Name: Benzene,1-(1,2-diphenyl-1-buten-1-yl)-4-methoxy-
• CAS No.: 69967-78-8
• Molecular Formula: C23H22 O
• Molecular Weight: 314.427

Synonyms:Anisole,p-(1,2-diphenyl-1-butenyl)- (7CI); Benzene,1-(1,2-diphenyl-1-butenyl)-4-methoxy- (9CI); 1-(4-Methoxyphenyl)-1,2-diphenyl-1-butene;ICI 90069

Chemical Property of Benzene,1-(1,2-diphenyl-1-buten-1-yl)-4-methoxy-

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of Benzene,1-(1,2-diphenyl-1-buten-1-yl)-4-methoxy-

There total 16 articles about Benzene,1-(1,2-diphenyl-1-buten-1-yl)-4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(3RS,4SR)-4-(4-methoxyphenyl)-3,4-diphenylbut-1-ene → (1-(4-methoxyphenyl)but-1-ene-1,2-diyl)dibenzene (69967-78-8)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 0.25h;

DOI:10.1016/j.bmc.2007.09.008

Reference yield: 96.0%

4-(4-methoxyphenyl)-3,4-diphenylbut-1-ene (650624-48-9) → (1-(4-methoxyphenyl)but-1-ene-1,2-diyl)dibenzene (69967-78-8)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 0.25h;

DOI:10.1016/j.tetlet.2003.11.119

Reference yield: 64.0%

1-((Z)-1,2-Diphenyl-buta-1,3-dienyl)-4-methoxy-benzene (857085-82-6) → (1-(4-methoxyphenyl)but-1-ene-1,2-diyl)dibenzene (69967-78-8)

Guidance literature:

With hydrogen; RhCl(PPh₃)3; In benzene; at 20 ℃;

DOI:10.1055/s-2004-836033

upstream raw materials:

bromobenzene

1-(4-methoxyphenyl)-2-phenylbutan-1-one

4-Methoxybenzophenone

1-phenyl-propan-1-one

Downstream raw materials:

1-(4-hydroxyphenyl)-1,2-diphenylbut-1-ene

tamoxifen

(E)-tamoxifen

N-demethyltamoxifen

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