Benzene, 1-(1,2-diphenyl-3-butenyl)-4-methoxy-

Base Information

Chemical Name:Benzene, 1-(1,2-diphenyl-3-butenyl)-4-methoxy-
CAS No.:650624-48-9
Molecular Formula:C23H22O
Molecular Weight:314.427
Hs Code.:
DSSTox Substance ID:DTXSID80469530
Nikkaji Number:J1.732.462D

Synonyms:Benzene, 1-(1,2-diphenyl-3-butenyl)-4-methoxy-;650624-48-9;DTXSID80469530

Suppliers and Price of Benzene, 1-(1,2-diphenyl-3-butenyl)-4-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzene, 1-(1,2-diphenyl-3-butenyl)-4-methoxy-

Chemical Property:

XLogP3:6.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:6
Exact Mass:314.167065321
Heavy Atom Count:24
Complexity:356

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C(C2=CC=CC=C2)C(C=C)C3=CC=CC=C3

Technology Process of Benzene, 1-(1,2-diphenyl-3-butenyl)-4-methoxy-

There total 1 articles about Benzene, 1-(1,2-diphenyl-3-butenyl)-4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 40595-34-4
(E)-trimethyl(3-phenylallyl)silane

: 100-52-7
benzaldehyde

: 100-66-3
methoxybenzene

: 4-(2-methoxyphenyl)-3,4-diphenylbut-1-ene

: 650624-48-9
4-(4-methoxyphenyl)-3,4-diphenylbut-1-ene

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; hafnium tetrachloride; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2007.09.008

Reference yield: 96.0%

: 650624-48-9
4-(4-methoxyphenyl)-3,4-diphenylbut-1-ene

: 69967-78-8
(1-(4-methoxyphenyl)but-1-ene-1,2-diyl)dibenzene

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 0.25h;
DOI:10.1016/j.tetlet.2003.11.119

Reference yield:

: 650624-48-9
4-(4-methoxyphenyl)-3,4-diphenylbut-1-ene

: 10540-29-1,7728-73-6
tamoxifen

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / t-BuOK / dimethylsulfoxide / 0.25 h / 20 °C

2: 98 percent / BBr₃ / CH₂Cl₂ / 2 h / -78 °C

3: 51 percent / dimethylformamide / 0.5 h / 50 °C

With potassium tert-butylate; boron tribromide; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2003.11.119