Benzenepropanoic acid, b-(acetyloxy)-, ethyl ester, (S)-

Base Information

Chemical Name:Benzenepropanoic acid, b-(acetyloxy)-, ethyl ester, (S)-
CAS No.:17126-70-4
Molecular Formula:C13H16O4
Molecular Weight:236.268
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanoic acid, b-(acetyloxy)-, ethyl ester, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzenepropanoic acid, b-(acetyloxy)-, ethyl ester, (S)-

There total 10 articles about Benzenepropanoic acid, b-(acetyloxy)-, ethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 25409-25-0
ethyl 3-acetoxy-3-phenylpropionate

: 72656-47-4
ethyl (R)-3-hydroxy-3-phenylpropanoate

: 17126-70-4
ethyl (S)-3-acetoxy-3-phenylpropanoate

Guidance literature:: With Saccharomyces cerrvisatae (ATCC 9080); In water; at 20 ℃; for 48h; Reagent/catalyst; Enzymatic reaction;
DOI:10.1016/j.tetasy.2013.09.007

Reference yield:

: 100-52-7
benzaldehyde

: 17126-70-4
ethyl (S)-3-acetoxy-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / 0.83 h / -78 °C

1.2: 0.5 h / -78 °C

2.1: Pseudomonas cepacia lipase (PS-C type II from Amano); tBuOMe / Ru catalyst / 144 h / 60 °C / Enzymatic reaction

With tert-butyl methyl ether; Pseudomonas cepacia lipase (PS-C type II from Amano); lithium diisopropyl amide; Ru catalyst; In tetrahydrofuran;
DOI:10.1021/ol015682p

Reference yield:

: 876-27-7
4-chlorophenyl acetate

: 5764-85-2
Ethyl 3-hydroxy-3-phenylpropanoate

: 37504-79-3
(R)-ethyl 3-acetoxy-3-phenylpropanoate

: 17126-70-4
ethyl (S)-3-acetoxy-3-phenylpropanoate

Guidance literature:: With tert-butyl methyl ether; Pseudomonas cepacia lipase (PS-C type II from Amano); Ru catalyst; at 60 ℃; for 144h; Title compound not separated from byproducts.; Enzymatic reaction;
DOI:10.1021/ol015682p