Hydrazinecarboxamide, N-(2,6-dichlorophenyl)-

Base Information

• Chemical Name: Hydrazinecarboxamide, N-(2,6-dichlorophenyl)-
• CAS No.: 171277-85-3
• Molecular Formula: C7H7Cl2N3O
• Molecular Weight: 220.058
• Mol file: 171277-85-3.mol

Synonyms:

Chemical Property of Hydrazinecarboxamide, N-(2,6-dichlorophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Hydrazinecarboxamide, N-(2,6-dichlorophenyl)-

There total 2 articles about Hydrazinecarboxamide, N-(2,6-dichlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,6-dichlorophenylisocyanate (39920-37-1) → C7H7Cl2N3O (171277-85-3)

Guidance literature:

With water; hydrazine; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/ja8019214

Reference yield: 98.0%

2,6-dichlorophenylisocyanate (39920-37-1) + hydrazine (302-01-2,78206-91-4,119775-10-9,75013-58-0) → C7H7Cl2N3O (171277-85-3)

Guidance literature:

In dichloromethane; water; at 20 ℃; Cooling with ice;

Reference yield: 96.0%

C7H7Cl2N3O (171277-85-3) + p-chlorphenylisocyanate (104-12-1) → C14H11Cl3N4O2 (1045820-46-9)

Guidance literature:

In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/ja8019214

upstream raw materials:

2,6-dichlorophenylisocyanate

hydrazine

Downstream raw materials:

C₁₅H₁₁Cl₂N₅O₂

C₁₄H₁₁Cl₃N₄O₂

Refernces

• 1、 -. "NOVEL AZOLES AND RELATED DERIVATIVES AS NON-NUCLEOSIDE REVERSE TRANSCRIPTASE INHIBITORS (NNRTIS) IN ANTIVIRAL THERAPY (HIV)". Page/Page column 28-29. . Retrieved 2009/03/07.