1,1'-(Diazidomethylene)dibenzene

Base Information

Chemical Name:1,1'-(Diazidomethylene)dibenzene
CAS No.:17421-82-8
Molecular Formula:C13H10N6
Molecular Weight:250.263
Hs Code.:
DSSTox Substance ID:DTXSID20566118
Nikkaji Number:J1.453.756B
Wikidata:Q82451579

Synonyms:17421-82-8;SCHEMBL20484507;DTXSID20566118;1,1'-(Diazidomethylene)dibenzene

Suppliers and Price of 1,1'-(Diazidomethylene)dibenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,1'-(Diazidomethylene)dibenzene

Chemical Property:

XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:250.09669434
Heavy Atom Count:19
Complexity:344

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(C2=CC=CC=C2)(N=[N+]=[N-])N=[N+]=[N-]

Technology Process of 1,1'-(Diazidomethylene)dibenzene

There total 7 articles about 1,1'-(Diazidomethylene)dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 119-61-9
benzophenone

: 7477-73-8
1,5-diphenyltetrazole

: 17421-82-8
diazido(diphenyl)methane

Guidance literature:: With sodium azide; titanium tetrachloride; In acetonitrile; for 17h; Ambient temperature;
DOI:10.1055/s-1993-26027

Reference yield:

: 119-61-9
benzophenone

: 17421-82-8
diazido(diphenyl)methane

Guidance literature:: Multi-step reaction with 3 steps

1: H₂SO₄ / methanol

2: N₂O₄, NaOAc / CH₂Cl₂

3: silica gel

With sulfuric acid; sodium acetate; silica gel; dinitrogen tetraoxide; In methanol; dichloromethane;
DOI:10.1021/jo00940a011

Reference yield:

: 52919-86-5
N'-(diphenylmethylene)acetohydrazide

: 17421-82-8
diazido(diphenyl)methane

Guidance literature:: Multi-step reaction with 2 steps

1: N₂O₄, NaOAc / CH₂Cl₂

2: silica gel

With sodium acetate; silica gel; dinitrogen tetraoxide; In dichloromethane;
DOI:10.1021/jo00940a011