Benzoic acid, 4-[[(4-chlorophenyl)methyl]amino]-3-nitro-, methyl ester

Base Information

Chemical Name:Benzoic acid, 4-[[(4-chlorophenyl)methyl]amino]-3-nitro-, methyl ester
CAS No.:174422-22-1
Molecular Formula:C15H13ClN2O4
Molecular Weight:320.732
Hs Code.:

Synonyms:methyl 4-(p-chlorobenzylamino)-3-nitro-benzoate;4-(4-Chloro-benzylamino)-3-nitro-benzoic acid methyl ester;methyl 4-((4-chlorobenzyl)amino)-3-nitrobenzoate;methyl 4-{[(4-chlorophenyl)methyl]amino}-3-nitrobenzoate;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 4-[[(4-chlorophenyl)methyl]amino]-3-nitro-, methyl ester

Chemical Property:

Melting Point:142 °C
PSA：84.15000
LogP:4.24310

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzoic acid, 4-[[(4-chlorophenyl)methyl]amino]-3-nitro-, methyl ester

There total 5 articles about Benzoic acid, 4-[[(4-chlorophenyl)methyl]amino]-3-nitro-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 329-59-9
4-fluoro-3-nitro-benzoic acid methyl ester

: 104-86-9
4-chlorobenzylamine

: 174422-22-1
methyl 4-(4-chlorobenzylamine)-3-nitrobenzoic acid ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 5h;

Reference yield: 89.0%

: 14719-83-6
methyl 3-nitro-4-chlorobenzoate

: 104-86-9
4-chlorobenzylamine

: 174422-22-1
methyl 4-(4-chlorobenzylamine)-3-nitrobenzoic acid ester

Guidance literature:: In tetrahydrofuran; at 40 ℃; for 2h;
DOI:10.1515/HC.2001.7.5.455

Reference yield:

: 453-71-4
3-nitro-4-fluorobenzoic acid

: 174422-22-1
methyl 4-(4-chlorobenzylamine)-3-nitrobenzoic acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 24 h / Reflux

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 17 h / Reflux

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2011.06.088