6H-Pyridazino[1,2-a][1,2]diazepine-1-carboxylic acid, octahydro-6,10-dioxo-9-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl ester, (1S,9S)-

Base Information

Chemical Name:6H-Pyridazino[1,2-a][1,2]diazepine-1-carboxylic acid, octahydro-6,10-dioxo-9-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl ester, (1S,9S)-
CAS No.:174799-31-6
Molecular Formula:C22H29N3O6
Molecular Weight:431.489
Hs Code.:

6H-Pyridazino[1,2-a][1,2]diazepine-1-carboxylic acid,
octahydro-6,10-dioxo-9-[[(phenylmethoxy)carbonyl]amino]-,
1,1-dimethylethyl ester, (1S,9S)-

Synonyms:

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Chemical Property of 6H-Pyridazino[1,2-a][1,2]diazepine-1-carboxylic acid, octahydro-6,10-dioxo-9-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl ester, (1S,9S)-

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Technology Process of 6H-Pyridazino[1,2-a][1,2]diazepine-1-carboxylic acid, octahydro-6,10-dioxo-9-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl ester, (1S,9S)-

There total 2 articles about 6H-Pyridazino[1,2-a][1,2]diazepine-1-carboxylic acid, octahydro-6,10-dioxo-9-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl ester, (1S,9S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 88767-96-8
(1S,9S)-t-butyl 9-amino-octahydro-6,10-dioxo-6H-pyridazino<1,2-a><1,2>diazepine-1-carboxylate

: 174799-31-6
(1S,9S)-tert-butyl 9-(benzyloxycarbonylamino)-6,10-dioxooctahydro-1H-pyridazino[1,2-a][1,2]diazepine-1-carboxylate

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 6h;

Reference yield:

: 106928-72-7
(1S,9S)-t-butyl 1,2,3,4,7,8,9,10-octahydro-6,10-dioxo-9-phthalimidopyridazino<1,2-a><1,2>diazepine-1-carboxylate

: 174799-31-6
(1S,9S)-tert-butyl 9-(benzyloxycarbonylamino)-6,10-dioxooctahydro-1H-pyridazino[1,2-a][1,2]diazepine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol / 3 h / 20 °C

2: sodium carbonate / N,N-dimethyl-formamide / 6 h / 0 - 20 °C

With sodium carbonate; hydrazine; In ethanol; N,N-dimethyl-formamide;