2-Propen-1-yl 3-(dimethylphenylsilyl)-4-methylpentanoate

Base Information

Chemical Name:2-Propen-1-yl 3-(dimethylphenylsilyl)-4-methylpentanoate
CAS No.:178940-42-6
Molecular Formula:C₁₇H₂₆O₂Si
Molecular Weight:290.478
Hs Code.:
DSSTox Substance ID:DTXSID401201605

Synonyms:DTXSID401201605;2-Propen-1-yl 3-(dimethylphenylsilyl)-4-methylpentanoate;178940-42-6

Suppliers and Price of 2-Propen-1-yl 3-(dimethylphenylsilyl)-4-methylpentanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propen-1-yl 3-(dimethylphenylsilyl)-4-methylpentanoate

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:8
Exact Mass:290.170206602
Heavy Atom Count:20
Complexity:317

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)C(CC(=O)OCC=C)[Si](C)(C)C1=CC=CC=C1

Technology Process of 2-Propen-1-yl 3-(dimethylphenylsilyl)-4-methylpentanoate

There total 6 articles about 2-Propen-1-yl 3-(dimethylphenylsilyl)-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 114431-82-2
methyl (3RS)-3-dimethyl(phenyl)silyl-4-methylpentanoate

: 107-18-6
allyl alcohol

: 178940-42-6
allyl 4-methyl-3-dimethyl(phenyl)silylpentanoate

Guidance literature:: With sulfuric acid; Heating;
DOI:10.1039/b305881f

Reference yield:

: 20515-15-5
methyl (2E)-4-methylpent-2-enoate

: 178940-42-6
allyl 4-methyl-3-dimethyl(phenyl)silylpentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) CuCN / 1.) 0 deg C, 1 h, 2.) THF, -78 deg C, 3 h

2: 95 percent / aq. LiOH / tetrahydrofuran; methanol / Heating

3: (COCl)2 / CH₂Cl₂ / 2 h / Ambient temperature

4: Et₃N / diethyl ether / 1 h

With lithium hydroxide; oxalyl dichloride; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1039/p19960001171

Reference yield:

: 3839-31-4
dimethyl(phenyl)silyllithium

: 178940-42-6
allyl 4-methyl-3-dimethyl(phenyl)silylpentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) CuCN / 1.) 0 deg C, 1 h, 2.) THF, -78 deg C, 3 h

2: 95 percent / aq. LiOH / tetrahydrofuran; methanol / Heating

3: (COCl)2 / CH₂Cl₂ / 2 h / Ambient temperature

4: Et₃N / diethyl ether / 1 h

With lithium hydroxide; oxalyl dichloride; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1039/p19960001171