Nα,1-Bis(trimethylsilyl)-L-histidine trimethylsilyl ester

Base Information

• Chemical Name: Nα,1-Bis(trimethylsilyl)-L-histidine trimethylsilyl ester
• CAS No.: 17908-25-7
• Molecular Formula: C15H33N3O2Si3
• Molecular Weight: 371.69800
• Mol file: 17908-25-7.mol

Synonyms:

Chemical Property of Nα,1-Bis(trimethylsilyl)-L-histidine trimethylsilyl ester

Chemical Property:

• Boiling Point: 115 °C (0.01 mmHg)
• PSA: 56.15000
• LogP: 3.67070

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Nα,1-Bis(trimethylsilyl)-L-histidine trimethylsilyl ester

There total 2 articles about Nα,1-Bis(trimethylsilyl)-L-histidine trimethylsilyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) + L-histidine (71-00-1,26062-48-6,90081-11-1) → 1,Nα-bis-trimethylsilanyl-histidine trimethylsilanyl ester (17908-25-7)

Guidance literature:

1,1,1,3,3,3-hexamethyl-disilazane; With sulfuric acid; for 0.0833333h;

L-histidine; for 0.666667h; Reflux;

Reference yield:

→ N,N'-Trimethylsilyl-histidin-trimethylsilylester (17908-25-7)

Guidance literature:

Histidin, N-Trimetylsilyl-diaethylamin, Δ;

upstream raw materials:

1,1,1,3,3,3-hexamethyl-disilazane

L-histidine

Refernces