6-fluorochrysene

Base Information

Chemical Name:6-fluorochrysene
CAS No.:3799-55-1
Molecular Formula:C₁₈H₁₁F
Molecular Weight:246.284
Hs Code.:

Synonyms:6-Fluorochrysene;NSC 80184

Suppliers and Price of 6-fluorochrysene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 6-fluorochrysene

Chemical Property:

Vapor Pressure:1.61E-07mmHg at 25°C
Boiling Point:439.7°C at 760 mmHg
Flash Point:185.6°C
Density:1.256g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-fluorochrysene

There total 14 articles about 6-fluorochrysene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1-(2-fluoro-2-phenylvinyl)naphthalene

: 3799-55-1
6-fluorochrysene

Guidance literature:: With iodine; methyloxirane; In benzene; for 8h; Inert atmosphere; Irradiation;
DOI:10.1021/acs.joc.5b02580

Reference yield: 51.0%

: 1-(2,2-difluorovinyl)-2-phenylnaphthalene

: 3799-55-1
6-fluorochrysene

Guidance literature:: With dimethylsulfide borane complex; silver trifluoromethanesulfonate; palladium dichloride; at 0 - 60 ℃; for 2h;
DOI:10.1021/ol503759d

Reference yield:

: 90-15-3
α-naphthol

: 3799-55-1
6-fluorochrysene

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-Bromosuccinimide; diisopropylamine / dichloromethane / 23 h / 20 °C / Reflux

2.1: pyridine / dichloromethane / 4 h / 0 - 20 °C

3.1: potassium phosphate; bis-triphenylphosphine-palladium(II) chloride; lithium bromide / toluene / 22 h / 20 °C / Reflux

4.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran; diethyl ether; cyclohexane; hexane / 0.33 h / -110 °C

4.2: 0.5 h / -100 °C

4.3: 16.5 h / Reflux

5.1: dimethylsulfide borane complex; silver trifluoromethanesulfonate; palladium dichloride / 2 h / 0 - 60 °C

With pyridine; bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; N-Bromosuccinimide; N,N,N,N,-tetramethylethylenediamine; dimethylsulfide borane complex; sec.-butyllithium; silver trifluoromethanesulfonate; diisopropylamine; lithium bromide; palladium dichloride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; cyclohexane; toluene;
DOI:10.1021/ol503759d