Bismuthonium, (1Z)-triphenyl-1-propenyl-, tetrafluoroborate(1-)

Base Information

Chemical Name:Bismuthonium, (1Z)-triphenyl-1-propenyl-, tetrafluoroborate(1-)
CAS No.:182330-22-9
Molecular Formula:BF₄*C₂₁H₂₀Bi
Molecular Weight:568.175
Hs Code.:
Mol file:182330-22-9.mol

Synonyms:

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Chemical Property of Bismuthonium, (1Z)-triphenyl-1-propenyl-, tetrafluoroborate(1-)

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Technology Process of Bismuthonium, (1Z)-triphenyl-1-propenyl-, tetrafluoroborate(1-)

There total 2 articles about Bismuthonium, (1Z)-triphenyl-1-propenyl-, tetrafluoroborate(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 109-63-7
trifluoroborane diethyl ether

: 4964-06-1,4964-07-2,17680-03-4
(E)-prop-1-enyl(trimethyl)stannane

: 2023-48-5,28719-53-1
triphenylbismuth(V) difluoride

: 182330-22-9,182330-20-7
(E)-prop-1-enyl(triphenyl)bismuthonium tetrafluoroborate

Guidance literature:: With Me₃SiCN; In dichloromethane; B-compd. and Si-compd. addn. to ice-cooled Bi-compd. soln., Sn-compd. addn. after 2 h, mixt. stirring 12 h at room temp., solvent evapn. under reduced pressure, residue short column chromy. (CH2Cl2), eluate evapn. under reduced pressure; residue crystn. (Et2O/CH2Cl2 10:1); elem. anal.;
DOI:10.1039/p19960001971

Reference yield:

: 109-63-7
trifluoroborane diethyl ether

: 2023-48-5,28719-53-1
triphenylbismuth(V) difluoride

: 4964-03-8
(E)-trimethyl(prop-1-en-1-yl)silane

: 182330-22-9,182330-20-7
(E)-prop-1-enyl(triphenyl)bismuthonium tetrafluoroborate

Guidance literature:: In dichloromethane; B-compd. and Si-compd. addn. to ice-cooled Bi-compd. soln., mixt. refluxing gently for 20 h, solvent evapn. under reduced pressure, residue washing (hexane); fractional crystn. from Et2O/CH2Cl2 1:1, mother liquor concn., passing through short silica gel column (CH2Cl2); elem. anal.;
DOI:10.1039/p19960001971