Benzoyl azide, 2-[(4-methoxyphenyl)thio]-

Base Information

Chemical Name:Benzoyl azide, 2-[(4-methoxyphenyl)thio]-
CAS No.:183583-30-4
Molecular Formula:C14H11N3O2S
Molecular Weight:285.326
Hs Code.:
DSSTox Substance ID:DTXSID30444498

Synonyms:Benzoyl azide, 2-[(4-methoxyphenyl)thio]-;183583-30-4;DTXSID30444498

Suppliers and Price of Benzoyl azide, 2-[(4-methoxyphenyl)thio]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzoyl azide, 2-[(4-methoxyphenyl)thio]-

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:285.05719778
Heavy Atom Count:20
Complexity:377

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)SC2=CC=CC=C2C(=O)N=[N+]=[N-]

Technology Process of Benzoyl azide, 2-[(4-methoxyphenyl)thio]-

There total 2 articles about Benzoyl azide, 2-[(4-methoxyphenyl)thio]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 43183-12-6
2-(4-Methoxyphenylthio)benzoyl chloride

: 183583-30-4
2-<(4-methoxyphenyl)thio>benzoyl azide

Guidance literature:: With sodium azide; In acetone; at 0 ℃; for 1h; Yield given;
DOI:10.1021/jm991005d

Reference yield:

: 19862-91-0
2-<(4-methoxyphenyl)thio>benzoic acid

: 183583-30-4
2-<(4-methoxyphenyl)thio>benzoyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / dimethylformamide / 1 h / Heating

2: 20 percent aq. NaN₃ / acetone / 1 h / 0 °C

With thionyl chloride; sodium azide; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm991005d