Ethanol, 2-(methyl(4-(2-(4-nitrophenyl)ethenyl)phenyl)amino)-

Base Information

• Chemical Name: Ethanol, 2-(methyl(4-(2-(4-nitrophenyl)ethenyl)phenyl)amino)-
• CAS No.: 122008-76-8
• Molecular Formula: C17H18 N2 O3
• Molecular Weight: 298.3364
• Nikkaji Number: J713.124K,J740.423I
• Mol file: 122008-76-8.mol

Synonyms:4-N-2-Hydroxyethyl-N-methylamino-4'-nitrostilbene;Stilbene, 4-N-2-hydroxyethyl-N-methylamino-4'-nitro-;Ethanol, 2-(methyl(4-(2-(4-nitrophenyl)ethenyl)phenyl)amino)-;122008-76-8;Ethanol, 2-[methyl[4-[2-(4-nitrophenyl)ethenyl]phenyl]amino]-;SCHEMBL3038695;2-[Methyl(4'-nitro-trans-stilbene-4-yl)amino]ethanol;2-[[4-[(E)-2-(4-Nitrophenyl)vinyl]phenyl](methyl)amino]ethanol

Chemical Property of Ethanol, 2-(methyl(4-(2-(4-nitrophenyl)ethenyl)phenyl)amino)-

Chemical Property:

• Vapor Pressure: 5.55E-10mmHg at 25°C
• Boiling Point: 479°Cat760mmHg
• Flash Point: 243.5°C
• PSA: 69.29000
• Density: 1.261g/cm³
• LogP: 3.71690
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 298.13174244
• Heavy Atom Count: 22
• Complexity: 365

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(CCO)C1=CC=C(C=C1)C=CC2=CC=C(C=C2)[N+](=O)[O-]
• Isomeric SMILES: CN(CCO)C1=CC=C(C=C1)/C=C/C2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of Ethanol, 2-(methyl(4-(2-(4-nitrophenyl)ethenyl)phenyl)amino)-

There total 1 articles about Ethanol, 2-(methyl(4-(2-(4-nitrophenyl)ethenyl)phenyl)amino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.4%

4-nitrobenzeneacetic acid (104-03-0) + 4-(N-methyl-N-hydroxyethylamino)benzaldehyde (1201-91-8) → 4-(N-(2-hydroxyethyl)-N-methylamino)-4′-nitrostilbene (122008-76-8)

Guidance literature:

With piperidine; at 100 - 120 ℃; for 3h;

DOI:10.1016/j.saa.2007.07.064

Reference yield: 79.0%

4-(hexyloxy)-2,5-diiodophenol (357396-86-2) + 4-(N-(2-hydroxyethyl)-N-methylamino)-4′-nitrostilbene (122008-76-8) → [2-(4-Hexyloxy-2,5-diiodo-phenoxy)-ethyl]-methyl-{4-[(E)-2-(4-nitro-phenyl)-vinyl]-phenyl}-amine (637036-63-6)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 48h;

DOI:10.1039/b208190c

Reference yield: 72.0%

6-bromohexanoyl chloride (22809-37-6) + 4-(N-(2-hydroxyethyl)-N-methylamino)-4′-nitrostilbene (122008-76-8) → 2-(N-methyl-N-(4-nitrostilbene)-4′-amino)ethyl 6-bromohexanoate (1431570-40-9)

Guidance literature:

4-(N-(2-hydroxyethyl)-N-methylamino)-4′-nitrostilbene; With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.25h;

6-bromohexanoyl chloride; at 0 - 20 ℃; for 24h;

DOI:10.1021/ma400247h

upstream raw materials:

4-nitrobenzeneacetic acid

4-(N-methyl-N-hydroxyethylamino)benzaldehyde

Downstream raw materials:

[2-(4-Hexyloxy-2,5-diiodo-phenoxy)-ethyl]-methyl-{4-[(E)-2-(4-nitro-phenyl)-vinyl]-phenyl}-amine

[p-(N-methyl-N-hydroxyethyl)-p'-nitro-stilbene]-(methylenebenzophenone) ether

C₂₀H₂₀N₂O₃

C₂₉H₂₈Cl₃N₅O₆S