2-Furancarboxylic acid, 4-methyl-5-[(phenylmethoxy)methyl]-, phenylmethyl ester

Base Information

Chemical Name:2-Furancarboxylic acid, 4-methyl-5-[(phenylmethoxy)methyl]-, phenylmethyl ester
CAS No.:184868-94-8
Molecular Formula:C21H20O4
Molecular Weight:336.387
Hs Code.:
Mol file:184868-94-8.mol

Synonyms:

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Chemical Property of 2-Furancarboxylic acid, 4-methyl-5-[(phenylmethoxy)methyl]-, phenylmethyl ester

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Technology Process of 2-Furancarboxylic acid, 4-methyl-5-[(phenylmethoxy)methyl]-, phenylmethyl ester

There total 2 articles about 2-Furancarboxylic acid, 4-methyl-5-[(phenylmethoxy)methyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6141-57-7
methyl 3-methylfuran-2-carboxylate

: 184868-94-8
5-Benzyloxymethyl-4-methyl-furan-2-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / LiAlH₄ / tetrahydrofuran / 1 h / 0 °C

2: 1.) n-BuLi / 1.) THF, 0 deg C, 2.5 h, 2.) THF, -40 deg C, 1.25 h

3: 1.) NaH, 2.) n-Bu₄NI / 1.) DMF, 25 deg C, 1 h, 2.) DMF, 100 deg C, 18 h

With lithium aluminium tetrahydride; n-butyllithium; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran;
DOI:10.1016/0040-4020(96)00865-4

Reference yield:

: 100-39-0
benzyl bromide

: 130446-62-7
5-Hydroxymethyl-4-methyl-furan-2-carboxylic acid

: 184868-94-8
5-Benzyloxymethyl-4-methyl-furan-2-carboxylic acid benzyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; Yield given. Multistep reaction; 1.) DMF, 25 deg C, 1 h, 2.) DMF, 100 deg C, 18 h;
DOI:10.1016/0040-4020(96)00865-4