3-Pyridinecarboxylic acid, 6-[(2-amino-2-oxoethyl)thio]-4-(4-chlorophenyl)-5-cyano-1,4-dihydro-2- methyl-, ethyl ester

Base Information

Chemical Name:3-Pyridinecarboxylic acid, 6-[(2-amino-2-oxoethyl)thio]-4-(4-chlorophenyl)-5-cyano-1,4-dihydro-2- methyl-, ethyl ester
CAS No.:184945-33-3
Molecular Formula:C₁₈H₁₈ClN₃O₃S
Molecular Weight:391.878
Hs Code.:
Mol file:184945-33-3.mol

Synonyms:

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Chemical Property of 3-Pyridinecarboxylic acid, 6-[(2-amino-2-oxoethyl)thio]-4-(4-chlorophenyl)-5-cyano-1,4-dihydro-2- methyl-, ethyl ester

Chemical Property:

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Technology Process of 3-Pyridinecarboxylic acid, 6-[(2-amino-2-oxoethyl)thio]-4-(4-chlorophenyl)-5-cyano-1,4-dihydro-2- methyl-, ethyl ester

There total 7 articles about 3-Pyridinecarboxylic acid, 6-[(2-amino-2-oxoethyl)thio]-4-(4-chlorophenyl)-5-cyano-1,4-dihydro-2- methyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19411-80-4
2-(4-chlorophenylmethylene)acetoacetic acid ethyl ester

: 184945-33-3
6-carbamoylmethylsulfanyl-4-(4-chloro-phenyl)-5-cyano-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine / ethanol / 0.17 h / Heating

2.1: ethanol / Heating

3.1: ethanol / 0.08 h / Heating

3.2: HCl / ethanol

With piperidine; In ethanol;
DOI:10.1007/s10593-005-0156-x

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 184945-33-3
6-carbamoylmethylsulfanyl-4-(4-chloro-phenyl)-5-cyano-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: piperidine / ethanol / 0.17 h / Heating

2.1: ethanol / Heating

3.1: ethanol / 0.08 h / Heating

3.2: HCl / ethanol

With piperidine; In ethanol;
DOI:10.1007/s10593-005-0156-x

Reference yield:

: 141-97-9
ethyl acetoacetate

: 184945-33-3
6-carbamoylmethylsulfanyl-4-(4-chloro-phenyl)-5-cyano-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: piperidine / ethanol / 0.17 h / Heating

2.1: ethanol / Heating

3.1: ethanol / 0.08 h / Heating

3.2: HCl / ethanol

With piperidine; In ethanol;
DOI:10.1007/s10593-005-0156-x