4-(4-Chloro-phenyl)-5-cyano-6-mercapto-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester; compound with piperidine

Base Information

Chemical Name:4-(4-Chloro-phenyl)-5-cyano-6-mercapto-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester; compound with piperidine
CAS No.:148859-86-3
Molecular Formula:C₅H₁₁N*C₁₆H₁₅ClN₂O₂S
Molecular Weight:419.975
Hs Code.:

Synonyms:4-(4-Chloro-phenyl)-5-cyano-6-mercapto-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester; compound with piperidine

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Chemical Property of 4-(4-Chloro-phenyl)-5-cyano-6-mercapto-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester; compound with piperidine

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Technology Process of 4-(4-Chloro-phenyl)-5-cyano-6-mercapto-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester; compound with piperidine

There total 5 articles about 4-(4-Chloro-phenyl)-5-cyano-6-mercapto-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester; compound with piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 110-89-4
piperidine

: 7357-70-2
Cyanothioacetamide

: 19411-80-4
2-(4-chlorophenylmethylene)acetoacetic acid ethyl ester

: 148859-86-3
4-(4-Chloro-phenyl)-5-cyano-6-mercapto-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester; compound with piperidine

Guidance literature:: In ethanol;
DOI:10.1007/BF00505906

Reference yield: 46.0%

: 110-89-4
piperidine

: 39145-33-0
2-cyano-3-(4-chlorophenyl)-prop-2-enethioamide

: 141-97-9
ethyl acetoacetate

: 148859-86-3
4-(4-Chloro-phenyl)-5-cyano-6-mercapto-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester; compound with piperidine

Guidance literature:: In ethanol;
DOI:10.1007/BF00505906

Reference yield:

: 39145-33-0
2-cyano-3-(4-chlorophenyl)-prop-2-enethioamide

: 148859-86-3
4-(4-Chloro-phenyl)-5-cyano-6-mercapto-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid ethyl ester; compound with piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / acetic acid; ethanol / 5 h / Heating

2: ethanol

In ethanol; acetic acid;
DOI:10.1007/BF00505906