1H-Pyrrole-2,5-dicarboxylic acid, 3-hexyl-4-methyl-, 2-methyl 5-(phenylmethyl) ester

Base Information

Chemical Name:1H-Pyrrole-2,5-dicarboxylic acid, 3-hexyl-4-methyl-, 2-methyl 5-(phenylmethyl) ester
CAS No.:185621-32-3
Molecular Formula:C₂₁H₂₇NO₄
Molecular Weight:357.45
Hs Code.:

Synonyms:

Suppliers and Price of 1H-Pyrrole-2,5-dicarboxylic acid, 3-hexyl-4-methyl-, 2-methyl 5-(phenylmethyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1H-Pyrrole-2,5-dicarboxylic acid, 3-hexyl-4-methyl-, 2-methyl 5-(phenylmethyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-Pyrrole-2,5-dicarboxylic acid, 3-hexyl-4-methyl-, 2-methyl 5-(phenylmethyl) ester

There total 6 articles about 1H-Pyrrole-2,5-dicarboxylic acid, 3-hexyl-4-methyl-, 2-methyl 5-(phenylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2199-64-6
ethyl 3,5-dimethyl-4-formyl-1H-pyrrole-2-carboxylate

: 185621-32-3
Benzyl 4-hexyl-5-carbomethoxy-3-methylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran; diethyl ether / 0.5 h / Ambient temperature

2: 3 M aq. HCl / CH₂Cl₂ / 0.42 h

3: 99 percent / H₂ / 5percent Pd/C / ethyl acetate / 24 h / 2585.7 Torr

4: 96 percent / Na / 19 h / 90 °C / 16 Torr

5: 1.) SO₂Cl₂, 2.) AcONa / 1.) CCl₄, 8 h, 2.) 50 deg C, 5 h

With hydrogenchloride; sulfuryl dichloride; hydrogen; sodium acetate; sodium; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jp962209y

Reference yield:

: 185621-31-2
Ethyl 3,5-dimethyl-4-(1-hexenyl)pyrrole-2-carboxylate

: 185621-32-3
Benzyl 4-hexyl-5-carbomethoxy-3-methylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / H₂ / 5percent Pd/C / ethyl acetate / 24 h / 2585.7 Torr

2: 96 percent / Na / 19 h / 90 °C / 16 Torr

3: 1.) SO₂Cl₂, 2.) AcONa / 1.) CCl₄, 8 h, 2.) 50 deg C, 5 h

With sulfuryl dichloride; hydrogen; sodium acetate; sodium; palladium on activated charcoal; In ethyl acetate;
DOI:10.1021/jp962209y

Reference yield:

: 693-25-4
n-pentylmagnesium bromide

: 185621-32-3
Benzyl 4-hexyl-5-carbomethoxy-3-methylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran; diethyl ether / 0.5 h / Ambient temperature

2: 3 M aq. HCl / CH₂Cl₂ / 0.42 h

3: 99 percent / H₂ / 5percent Pd/C / ethyl acetate / 24 h / 2585.7 Torr

4: 96 percent / Na / 19 h / 90 °C / 16 Torr

5: 1.) SO₂Cl₂, 2.) AcONa / 1.) CCl₄, 8 h, 2.) 50 deg C, 5 h

With hydrogenchloride; sulfuryl dichloride; hydrogen; sodium acetate; sodium; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jp962209y