1,1'-[1,3-Phenylenebis(diazomethylene)]dibenzene

Base Information

• Chemical Name: 1,1'-[1,3-Phenylenebis(diazomethylene)]dibenzene
• CAS No.: 18615-40-2
• Molecular Formula: C20H14N4
• Molecular Weight: 310.358
• DSSTox Substance ID: DTXSID80518012
• Nikkaji Number: J1.645.158D

Synonyms:18615-40-2;1,3-bis(a-diazobenzyl)benzene;DTXSID80518012;1,1'-[1,3-Phenylenebis(diazomethylene)]dibenzene

Chemical Property of 1,1'-[1,3-Phenylenebis(diazomethylene)]dibenzene

Chemical Property:

• XLogP3: 5.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 310.121846464
• Heavy Atom Count: 24
• Complexity: 470

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=[N+]=[N-])C2=CC(=CC=C2)C(=[N+]=[N-])C3=CC=CC=C3

Technology Process of 1,1'-[1,3-Phenylenebis(diazomethylene)]dibenzene

There total 3 articles about 1,1'-[1,3-Phenylenebis(diazomethylene)]dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

[1-[3-(Hydrazono-phenyl-methyl)-phenyl]-1-phenyl-meth-(E)-ylidene]-hydrazine + methanol (67-56-1) → 1,3-dibenzoylbenzene bis-dimethyl acetal + 1,3-Bis(α-diazo-benzyl)benzene (18615-40-2)

Guidance literature:

With sodium methylate; potassium iodide; at 15 ℃; Electrolysis;

Reference yield:

1,3-Dibenzoyl-benzol-bis-hydrazon (36323-31-6) → 1,3-Bis(α-diazo-benzyl)benzene (18615-40-2)

Guidance literature:

With potassium hydroxide; mercury(II) oxide;

DOI:10.1016/0040-4020(72)88031-1

Reference yield:

→ 1,3-Bis(α-diazo-benzyl)benzene (18615-40-2)

Guidance literature:

1,3-Dibenzoyl-benzol-bis-hydrazon, MnO2, ethanol. KOH (Ae., unter Lichtausschluss);

DOI:10.1021/jo01028a513

upstream raw materials:

1,3-Dibenzoyl-benzol-bis-hydrazon

methanol

Downstream raw materials:

1,3-dibenzoylbenzene

1,3-dibenzylbenzene

Acetic acid [3-(acetoxy-phenyl-methyl)-phenyl]-phenyl-methyl ester

2,2'-<1,3-Phenylenbis(phenylmethylio)>bis(3,5-dioxo-4-phenyl-1,2,4-triazolidin-1-id)

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 18615-40-2 Benzene, 1,3-bis(diazophenylmethyl)-

Send

Send

Metric Ton KG G Pound L ML

Send

Send