2-AMINO-5-CHLORO-N'-PHENYLBENZOHYDRAZIDE

Base Information

• Chemical Name: 2-AMINO-5-CHLORO-N'-PHENYLBENZOHYDRAZIDE
• CAS No.: 18852-01-2
• Molecular Formula: C13H12ClN3O
• Molecular Weight: 261.711
• Mol file: 18852-01-2.mol

Synonyms:2-Amino-5-chloro-benzoic acid N'-phenyl-hydrazide;

Chemical Property of 2-AMINO-5-CHLORO-N'-PHENYLBENZOHYDRAZIDE

Chemical Property:

• Melting Point: 201 - 203 °C (ethanol)
• PSA: 67.15000
• LogP: 3.72420

Purity/Quality:

99% ^*data from raw suppliers

2-AMINO-5-CHLORO-N'-PHENYLBENZOHYDRAZIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 2-AMINO-5-CHLORO-N'-PHENYLBENZOHYDRAZIDE

There total 2 articles about 2-AMINO-5-CHLORO-N'-PHENYLBENZOHYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-Chloroisatoic anhydride (4743-17-3) + phenylhydrazine (100-63-0) → 2-Amino-5-chlor-N2-phenyl-benzoesaeure-hydrazid (18852-01-2)

Guidance literature:

In ethanol;

Reference yield:

→ 2-Amino-5-chlor-N2-phenyl-benzoesaeure-hydrazid (18852-01-2)

Guidance literature:

Aus 5-Chlorisatinsaeureanhydrid mit Phenylhydrazin;

Reference yield: 91.0%

1,7-dichloro-4-heptanone (40624-07-5) + 2-Amino-5-chlor-N2-phenyl-benzoesaeure-hydrazid (18852-01-2) → 7-chloro-3a-(3-chloropropyl)-4-(phenylamino)-2,3,3a,4-tetrahydropyrrolo[1,2-a]quinazolin-5(1H)-one

Guidance literature:

With iodine; sodium hydrogencarbonate; In acetonitrile; for 10h; Reflux;

DOI:10.1016/j.tet.2016.03.018

upstream raw materials:

5-Chloroisatoic anhydride

phenylhydrazine

Downstream raw materials:

C₁₅H₁₀ClN₅O

C₁₆H₁₂ClN₅O

C₁₇H₁₄ClN₅O

C₁₄H₁₂ClN₅O

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