Phenyl(2-phenyl-1,3-dioxolan-2-yl)methanone

Base Information

• Chemical Name: Phenyl(2-phenyl-1,3-dioxolan-2-yl)methanone
• CAS No.: 6252-00-2
• Molecular Formula: C16H14 O3
• Molecular Weight: 254.285
• NSC Number: 53723
• DSSTox Substance ID: DTXSID80287978
• Nikkaji Number: J2.105.976E
• Wikidata: Q82024213
• Mol file: 6252-00-2.mol

Synonyms:6252-00-2;phenyl(2-phenyl-1,3-dioxolan-2-yl)methanone;NSC53723;benzoylphenyldioxolane;ghl.PD_Mitscher_leg0.134;SCHEMBL1551316;DTXSID80287978;NSC-53723

Chemical Property of Phenyl(2-phenyl-1,3-dioxolan-2-yl)methanone

Chemical Property:

• Vapor Pressure: 1.63E-06mmHg at 25°C
• Boiling Point: 397°C at 760 mmHg
• Flash Point: 185.5°C
• PSA: 35.53000
• Density: 1.208g/cm³
• LogP: 2.76910
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 254.094294304
• Heavy Atom Count: 19
• Complexity: 308

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1COC(O1)(C2=CC=CC=C2)C(=O)C3=CC=CC=C3

Technology Process of Phenyl(2-phenyl-1,3-dioxolan-2-yl)methanone

There total 6 articles about Phenyl(2-phenyl-1,3-dioxolan-2-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

phenyl-(2-phenyl-[1,3]dioxolan-2-yl)-methanol (5694-69-9) → phenyl-(2-phenyl-1,3-dioxolan-2-yl)methanone (6252-00-2)

Guidance literature:

With N-Bromosuccinimide; In tetrachloromethane; for 15h; Heating;

DOI:10.1021/jo00231a026

Reference yield: 59.0%

ethylene glycol (107-21-1) + diphenyl acetylene (501-65-5) → phenyl-(2-phenyl-1,3-dioxolan-2-yl)methanone (6252-00-2)

Guidance literature:

With oxygen; 9-(2-mesityl)-10-methylacridinium perchlorate; In acetonitrile; at 25 ℃; for 3h; UV-irradiation; Green chemistry;

DOI:10.1039/c8gc02766h

Reference yield: 24.0%

di-isopropyl azodicarboxylate (2446-83-5) + phenyl-(2-phenyl-[1,3]dioxolan-2-yl)-methanol (5694-69-9) → phenyl-(2-phenyl-1,3-dioxolan-2-yl)methanone (6252-00-2) + C40H44N2O8 (110271-99-3)

Guidance literature:

With triphenylphosphine; In tetrahydrofuran; Ambient temperature;

DOI:10.1021/jo00231a026

upstream raw materials:

phenyl-(2-phenyl-[1,3]dioxolan-2-yl)-methanol

5,6-Diphenyl-2,3-dihydro-[1,4]dioxine

di-isopropyl azodicarboxylate

2-hydroxy-2-phenylacetophenone

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