3-ISOBUTYL-6-METHYL-2,5-PIPERAZINEDIONE

Base Information

• Chemical Name: 3-ISOBUTYL-6-METHYL-2,5-PIPERAZINEDIONE
• CAS No.: 1803-60-7
• Molecular Formula: C9H16 N2 O2
• Molecular Weight: 184.238
• Hs Code.: 2933599090
• Mol file: 1803-60-7.mol

Synonyms:2,5-Piperazinedione,3-isobutyl-6-methyl- (7CI,8CI); 3-Isobutyl-6-methylpiperazine-2,5-dione;Cyclo(alanylleucyl); Leucine, cyclic dipeptide with alanine

Chemical Property of 3-ISOBUTYL-6-METHYL-2,5-PIPERAZINEDIONE

Chemical Property:

• PSA: 58.20000
• LogP: 0.69320
• Storage Temp.: 2-8°C

Purity/Quality:

98%,99%, ^*data from raw suppliers

Cyclo(Leu-Ala) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 3-ISOBUTYL-6-METHYL-2,5-PIPERAZINEDIONE

There total 18 articles about 3-ISOBUTYL-6-METHYL-2,5-PIPERAZINEDIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

C2F6NO4S2(1-)*C38H50N3O6(1+) (905984-90-9) → C2F6NO4S2(1-)*C23H40N3O4(1+) (1256258-73-7) + (3S,6S)-3-methyl-6-(2-methylpropyl)piperazine-2,5-dione (1803-60-7,5845-58-9,5845-60-3,24676-83-3,35590-72-8,125410-18-6)

Guidance literature:

With piperidine; In acetonitrile; at 20 ℃; for 0.25h; Inert atmosphere;

DOI:10.1016/j.tet.2010.07.016

Reference yield: 85.0%

C2F6NO4S2(1-)*C33H48N3O5(1+) (1001249-92-8) → C2F6NO4S2(1-)*C18H38N3O3(1+) (1256258-71-5) + (3S,6S)-3-methyl-6-(2-methylpropyl)piperazine-2,5-dione (1803-60-7,5845-58-9,5845-60-3,24676-83-3,35590-72-8,125410-18-6)

Guidance literature:

With piperidine; In acetonitrile; at 20 ℃; for 0.25h; Inert atmosphere;

DOI:10.1016/j.tet.2010.07.016

Reference yield:

alanyl=>leucyl=>-glycine (82267-71-8) + β-naphthol (135-19-3) → glycine (56-40-6,18875-39-3,25718-94-9) + DL-alanyl-leucyl anhydride (1803-60-7)

Guidance literature:

at 135 - 150 ℃;

upstream raw materials:

methanol

DL-Leucyl-DL-alanine

D,L-alanyl-D,L-leucine

β-naphthol

Downstream raw materials:

rac-Ala-OH

LEUCINE

DL-Leucyl-DL-alanine

L-valine hydrochloride

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