2-Iodo-3-nitrobenzamide

Base Information

Chemical Name:2-Iodo-3-nitrobenzamide
CAS No.:189125-09-5
Molecular Formula:C₇H₅IN₂O₃
Molecular Weight:292.033
Hs Code.:
DSSTox Substance ID:DTXSID40443851
Nikkaji Number:J851.942K
Wikidata:Q82261824

Synonyms:2-iodo-3-nitrobenzamide;189125-09-5;Benzamide, 2-iodo-3-nitro-;2-Iodo-3-nitro benzamide;2-iodo-3 nitrobenzamide;3-Nitro-2-iodobenzamide;SCHEMBL434821;DTXSID40443851;AKOS026674244

Suppliers and Price of 2-Iodo-3-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Iodo-3-nitrobenzamide

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:291.93449
Heavy Atom Count:13
Complexity:228

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)[N+](=O)[O-])I)C(=O)N

Technology Process of 2-Iodo-3-nitrobenzamide

There total 3 articles about 2-Iodo-3-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1261481-69-9
C₇H₃IN₂O₂

: 189125-09-5
2-iodo-3-nitrobenzamide

Guidance literature:: With dihydrogen peroxide; sodium carbonate; In acetone; at 5 - 20 ℃; for 1h;
DOI:10.1007/s12039-012-0325-2

Reference yield:

: 87331-46-2
2-amino-3-nitrobenzonitrile

: 189125-09-5
2-iodo-3-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / water / 0.5 h / 0 - 5 °C

1.2: 4 h / 5 - 20 °C

2.1: dihydrogen peroxide; sodium carbonate / acetone / 1 h / 5 - 20 °C

With hydrogenchloride; dihydrogen peroxide; sodium carbonate; sodium nitrite; In water; acetone; 1.1: |Sandmeyer Reaction / 1.2: |Sandmeyer Reaction;
DOI:10.1007/s12039-012-0325-2