2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-pyridinyl)-

Base Information

Chemical Name:2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-pyridinyl)-
CAS No.:89659-91-6
Molecular Formula:C₁₃H₁₀ClN₃O
Molecular Weight:259.695
Hs Code.:
DSSTox Substance ID:DTXSID30237807
Wikidata:Q83120032

Synonyms:BRN 5281664;2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-pyridinyl)-;1-Methyl-3-(2-pyridyl)-5-chlorobenzimidazolin-2-one;89659-91-6;1,3-Dihydro-5-chloro-1-methyl-3-(2-pyridinyl)-2H-benzimidazol-2-one;DTXSID30237807;LS-33332

Suppliers and Price of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-pyridinyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-pyridinyl)-

Chemical Property:

Vapor Pressure:1.42E-07mmHg at 25°C
Boiling Point:429.3°Cat760mmHg
Flash Point:213.4°C
Density:1.392g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:259.0512396
Heavy Atom Count:18
Complexity:338

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)Cl)N(C1=O)C3=CC=CC=N3

Technology Process of 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-pyridinyl)-

There total 4 articles about 2H-Benzimidazol-2-one, 1,3-dihydro-5-chloro-1-methyl-3-(2-pyridinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 89659-90-5
3-(2-pyridyl)-5-chlorobenzimidazolin-2-one

: 74-88-4
methyl iodide

: 89659-91-6
1-methyl-3-(2-pyridyl)-5-chlorobenzimidazolin-2-one

Guidance literature:: With potassium carbonate; In methanol; for 2h; Heating;

Reference yield:

: 89660-11-7
N-(5-chloro-2-nitrophenyl)pyridin-2-amine

: 89659-91-6
1-methyl-3-(2-pyridyl)-5-chlorobenzimidazolin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / H₂ / PtO₂ / aq. ethanol / 35 - 40 °C / 760 Torr

2: 75 percent / CHCl₃ / 4 h / Heating

3: 64 percent / EtONa / ethanol / 2 h / Heating

4: 81 percent / anhydrous K₂CO₃ / methanol / 2 h / Heating

With hydrogen; sodium ethanolate; potassium carbonate; platinum(IV) oxide; In methanol; ethanol; chloroform;

Reference yield:

: 74896-03-0
N¹-(2-pyridyl)-4-chloro-o-phenylenediamine

: 89659-91-6
1-methyl-3-(2-pyridyl)-5-chlorobenzimidazolin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / CHCl₃ / 4 h / Heating

2: 64 percent / EtONa / ethanol / 2 h / Heating

3: 81 percent / anhydrous K₂CO₃ / methanol / 2 h / Heating

With sodium ethanolate; potassium carbonate; In methanol; ethanol; chloroform;