Germane, dichloro-9H-fluoren-9-yl[2,4,6-tris(1-methylethyl)phenyl]-

Base Information

Chemical Name:Germane, dichloro-9H-fluoren-9-yl[2,4,6-tris(1-methylethyl)phenyl]-
CAS No.:190080-53-6
Molecular Formula:C₂₈H₃₂Cl₂Ge
Molecular Weight:512.058
Hs Code.:

Synonyms:

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Chemical Property of Germane, dichloro-9H-fluoren-9-yl[2,4,6-tris(1-methylethyl)phenyl]-

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Technology Process of Germane, dichloro-9H-fluoren-9-yl[2,4,6-tris(1-methylethyl)phenyl]-

There total 1 articles about Germane, dichloro-9H-fluoren-9-yl[2,4,6-tris(1-methylethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 190080-50-3
trichloro(2,4,6-triisopropylphenyl)germane

: 881-04-9
9H-fluoren-9-yllithium

: 190080-53-6
dichloro(fluorenyl)(2,4,6-triisopropylphenyl)germane

: lithium chloride

Guidance literature:: In tetrahydrofuran; high vac. techniques; addn. of soln. of fluorenyllithium to soln. of Ge compound (-78°C), warming to room temp., heating (65°C, 2 h); solvent removal (vac.), addn. of pentane, filtration off of LiCl, recrystn. (pentane); elem. anal.;
DOI:10.1080/00945719708000207

Reference yield: 81.0%

: 190080-53-6
dichloro(fluorenyl)(2,4,6-triisopropylphenyl)germane

: 7664-39-3,12381-92-9,32057-09-3,74835-82-8
hydrogen fluoride

: 190080-55-8
difluoro(fluorenyl)(2,4,6-triisopropylphenyl)germane

Guidance literature:: With triethylamine; In methanol; hydrogen fluoride; benzene; byproducts: Et3N*HCl; high vac. techniques; addn. of MeOH and Et3N to soln. of Ge compound in C6H6, heating (40°C, 30 min), cooling (15°C), filtration off of Et3N*HCl, addn. of aq. HF (40 %), stirring (room temp., 1 h); extn. into Et2O, drying (over Na2SO4), recrystn. (pentane); elem. anal.;
DOI:10.1080/00945719708000207

Reference yield: 61.0%

: 16853-85-3
lithium aluminium tetrahydride

: 190080-53-6
dichloro(fluorenyl)(2,4,6-triisopropylphenyl)germane

: 190080-54-7
fluorenyl(2,4,6-triisopropylphenyl)germane

Guidance literature:: With water; In diethyl ether; high vac. techniques; addn. of soln. of Ge compound to suspn. of (-10°C), -10°C (30 min), hydrolysis (0°C); org. phase sepd., drying (over Na2SO4), crystn. (pentane); elem. anal.;
DOI:10.1080/00945719708000207