Germane, trichloro[2,4,6-tris(1-methylethyl)phenyl]-

Base Information

Chemical Name:Germane, trichloro[2,4,6-tris(1-methylethyl)phenyl]-
CAS No.:190080-50-3
Molecular Formula:C15H23Cl3Ge
Molecular Weight:382.297
Hs Code.:

Synonyms:

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Chemical Property of Germane, trichloro[2,4,6-tris(1-methylethyl)phenyl]-

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Technology Process of Germane, trichloro[2,4,6-tris(1-methylethyl)phenyl]-

There total 2 articles about Germane, trichloro[2,4,6-tris(1-methylethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 21524-34-5
2,4,6-triisopropyl-1-bromobenzene

: 10038-98-9
germaniumtetrachloride

: 190080-50-3
trichloro(2,4,6-triisopropylphenyl)germane

Guidance literature:: 2,4,6-triisopropyl-1-bromobenzene; With magnesium; In tetrahydrofuran; for 2.5h; Reflux; Inert atmosphere;

With 1,4-dioxane; In tetrahydrofuran; for 0.0833333h; Reflux; Inert atmosphere;

germaniumtetrachloride; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere; Reflux;
DOI:10.1039/c5dt03918e

Reference yield: 76.0%

: 56-23-5
tetrachloromethane

: 190080-49-0
2,4,6-triisopropylphenylgermane

: 190080-50-3
trichloro(2,4,6-triisopropylphenyl)germane

Guidance literature:: With α,α'-azo-bis-isobutyronitril; In tetrachloromethane; benzene; high vac. techniques; addn. of soln. of Ge compound in C6H6 to suspn. ofAIBN in CCl4, refluxing (1 h); solvent removal (vac.), recrystn. (pentane); elem. anal.;
DOI:10.1080/00945719708000207

Reference yield: 87.0%

: 67-56-1
methanol

: 190080-50-3
trichloro(2,4,6-triisopropylphenyl)germane

: 438201-90-2
2,4,6-triisopropylphenyl(trimethoxy)germane

Guidance literature:: With triethylamine; In toluene; byproducts: Et3N*HCl; MeOH and Et3N were added to soln. of Ge-compound in toluene, refluxed for 1 h, warmed to room temp. under N2 or Ar; solvent was removed in vacuo, pentane was added, filtered off, pentane was removed; elem. anal.;
DOI:10.1016/S0022-328X(01)01223-2