4-(2-Hydroxyethyl)-4-methyl-1,3-dioxane

Base Information

• Chemical Name: 4-(2-Hydroxyethyl)-4-methyl-1,3-dioxane
• CAS No.: 2018-45-3
• Molecular Formula: C7H14 O3
• Molecular Weight: 146.186
• Hs Code.: 2932999099
• DSSTox Substance ID: DTXSID20942236
• Nikkaji Number: J25.348K
• Mol file: 2018-45-3.mol

Synonyms:4-methyl-4-hydroxyethyl-1,3-dioxane;4-methyl-4-hydroxyethyl-m-dioxane;MHEMD

Chemical Property of 4-(2-Hydroxyethyl)-4-methyl-1,3-dioxane

Chemical Property:

• Vapor Pressure: 0.029mmHg at 25°C
• Boiling Point: 217.1°Cat760mmHg
• Flash Point: 101.5°C
• PSA: 38.69000
• Density: 1.029g/cm³
• LogP: 0.52190
• XLogP3: 0.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 146.094294304
• Heavy Atom Count: 10
• Complexity: 105

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CCOCO1)CCO

Technology Process of 4-(2-Hydroxyethyl)-4-methyl-1,3-dioxane

There total 1 articles about 4-(2-Hydroxyethyl)-4-methyl-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 4-(β-hydroxyethyl)-4-methyl-1,3-dioxane (2018-45-3)

Guidance literature:

Aus Butenol I u. Formaldehyd;

DOI:10.1007/BF00923187

Reference yield: 65.0%

4-(β-hydroxyethyl)-4-methyl-1,3-dioxane (2018-45-3) → 3-methylpentane-1,5-diol (4457-71-0)

Guidance literature:

With hydrogen; copper; at 240 ℃; for 5h; under 225018 Torr;

Reference yield: 5.0%

4-(β-hydroxyethyl)-4-methyl-1,3-dioxane (2018-45-3) → 2-hydroxy-2-methylbutane-1,4-dioic acid (597-44-4,2306-22-1) + meglutol (503-49-1) + oxalic acid (144-62-7,97993-78-7)

Guidance literature:

With nitric acid; 1. adding, 7 h; 50-60 deg C, 1 h;

DOI:10.1007/BF00474057

Downstream raw materials:

3-methylpentane-1,5-diol

2-hydroxy-2-methylbutane-1,4-dioic acid

meglutol

oxalic acid