Cyclobutanecarbonitrile, 2,2-dimethyl-3-methylene-

Base Information

• Chemical Name: Cyclobutanecarbonitrile, 2,2-dimethyl-3-methylene-
• CAS No.: 30758-34-0
• Molecular Formula: C8H11 N
• Molecular Weight: 121.182
• Hs Code.: 2926909090
• DSSTox Substance ID: DTXSID80952972
• Nikkaji Number: J48.583G
• Mol file: 30758-34-0.mol

Synonyms:BRN 1928472;30758-34-0;USAF A-20164;2,2-dimethyl-3-methylidenecyclobutane-1-carbonitrile;CYCLOBUTANECARBONITRILE, 2,2-DIMETHYL-3-METHYLENE-;2,2-Dimethyl-3-methylenecyclobutane carbonitrile;4-09-00-00135 (Beilstein Handbook Reference);2,2-Dimethyl-3-methylenecyclobutane-1-carbonitrile;DTXSID80952972;LS-55833

Chemical Property of Cyclobutanecarbonitrile, 2,2-dimethyl-3-methylene-

Chemical Property:

• Vapor Pressure: 0.769mmHg at 25°C
• Boiling Point: 183.5°Cat760mmHg
• Flash Point: 57.5°C
• PSA: 23.79000
• Density: 0.91g/cm³
• LogP: 2.11228
• XLogP3: 1.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 121.089149355
• Heavy Atom Count: 9
• Complexity: 192

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(C(CC1=C)C#N)C

Technology Process of Cyclobutanecarbonitrile, 2,2-dimethyl-3-methylene-

There total 4 articles about Cyclobutanecarbonitrile, 2,2-dimethyl-3-methylene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dimethylallene (598-25-4) + acrylonitrile (107-13-1,25014-41-9) → 2,2-dimethyl-3-methylene-cyclobutanecarbonitrile (30758-34-0)

Guidance literature:

In benzene;

DOI:10.1021/ja00955a020

Reference yield:

Dimethylallene (598-25-4) + acrylonitrile (107-13-1,25014-41-9) → 2,2-dimethyl-3-methylene-cyclobutanecarbonitrile (30758-34-0) + 3-isopropylidene-cyclobutanecarbonitrile (30758-35-1)

Guidance literature:

DOI:10.1021/ja01520a033

Reference yield:

10H-phenothiazine (92-84-2) + Dimethylallene (598-25-4) + acrylonitrile (107-13-1,25014-41-9) → 2,2-dimethyl-3-methylene-cyclobutanecarbonitrile (30758-34-0) + 3-isopropylidene-cyclobutanecarbonitrile (30758-35-1)

Guidance literature:

at 200 ℃;

DOI:10.1021/ja01520a033

upstream raw materials:

10H-phenothiazine

Dimethylallene

acrylonitrile

Downstream raw materials:

2,2,4,4-Tetramethyl-3-cyanocyclobutyl-benzolsulfonat

Dimethylallene

5-methyl-4-methylene-hex-5-enenitrile

acrylonitrile