1,3,2-Dioxaborinane, 2-chloro-

Base Information

• Chemical Name: 1,3,2-Dioxaborinane, 2-chloro-
• CAS No.: 1003-43-6
• Molecular Formula: C3H6BClO2
• Molecular Weight: 120.343
• Mol file: 1003-43-6.mol

Synonyms:

Chemical Property of 1,3,2-Dioxaborinane, 2-chloro-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3,2-Dioxaborinane, 2-chloro-

There total 1 articles about 1,3,2-Dioxaborinane, 2-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trimethylenebis(oxyboryldichloride) (237739-28-5) → boron trichloride (10294-34-5) + 2-chloro-[1,3,2]dioxaborinane (1003-43-6)

Guidance literature:

room temp.;

Reference yield: 76.0%

diethylamine (109-89-7) + 2-chloro-[1,3,2]dioxaborinane (1003-43-6) → Borsaeure-diethylamid-trimethylenester (25031-69-0)

Guidance literature:

DOI:10.1039/jr9620001428

Reference yield:

Methyltriphenylphosphonium bromide (1779-49-3) + 2-chloro-[1,3,2]dioxaborinane (1003-43-6) → [(1,3,2-dioxaborin-2-yl)methylene]triphenylphosphorane (83947-64-2)

Guidance literature:

With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; Ph3(Me)PBr in THF was treated with BuLi (25°C, Ar), stirred 30 min, cooled to -78°C, a THF soln. of borinane was added, mixt. wasstirred for 10 min at -78°C, warmed to 0°C, treated with LDA in THF, stirred 1 h at 0°C; not isolated from the soln.;

DOI:10.1021/om00074a005

upstream raw materials:

trimethylenebis(oxyboryldichloride)

Downstream raw materials:

Borsaeure-diethylamid-trimethylenester

2-n-butyl-1,3,2-dioxaborinane

Borsaeure-tris-<3-chlor-propylester>

((CH₂)3O₂)B(O-cyclo-C₆H₁₁)