5,5'-Dichloro-2,2'-dimethylazoxybenzene

Base Information

• Chemical Name: 5,5'-Dichloro-2,2'-dimethylazoxybenzene
• CAS No.: 66941-45-5
• Molecular Formula: C14H12Cl2N2O
• Molecular Weight: 295.168
• Mol file: 66941-45-5.mol

Synonyms:2.2'-Dimethyl-5.5'-dichlor-azoxybenzol;5,5'-Dichlor-2,2'-dimethyl-azobenzol;AZOXYBENZENE,5,5'-DICHLORO-2,2'-DIMETHYL;Dichloro-5,5' dimethyl-2,2' azoxybenzene;5.5'-Dichlor-2.2'-dimethyl-azoxybenzol;

Chemical Property of 5,5'-Dichloro-2,2'-dimethylazoxybenzene

Chemical Property:

• Vapor Pressure: 6.98E-08mmHg at 25°C
• Boiling Point: 450.5°Cat760mmHg
• Flash Point: 226.3°C
• PSA: 41.11000
• Density: 1.27g/cm³
• LogP: 6.05910

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,5'-Dichloro-2,2'-dimethylazoxybenzene

There total 4 articles about 5,5'-Dichloro-2,2'-dimethylazoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-2-nitrotoluene (89-59-8) → 5-chloro-2-methyl-benzenamine (95-79-4) + bis-(5-chloro-2-methyl-phenyl)-diazene-N-oxide (66941-45-5)

Guidance literature:

With sodium ethanolate; benzene;

DOI:10.1021/ja01357a050

Reference yield:

4-chloro-2-nitrotoluene (89-59-8) + sodium ethanolate (141-52-6) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 5-chloro-2-methyl-benzenamine (95-79-4) + bis-(5-chloro-2-methyl-phenyl)-diazene-N-oxide (66941-45-5)

Guidance literature:

DOI:10.1021/ja01357a050

Reference yield:

4-chloro-2-nitrotoluene (89-59-8) → bis-(5-chloro-2-methyl-phenyl)-diazene-N-oxide (66941-45-5)

Guidance literature:

With sodium; und behandelt das schwarze Reaktionsprodukts mit Salzsaeure;

upstream raw materials:

4-chloro-2-nitrotoluene

sodium ethanolate

benzene

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