Adenosine, 3'-deoxy-N-[[2-(4-nitrophenyl)ethoxy]carbonyl]-, 5'-[6-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]hexanoate] 2'-[2-(4-nitrophenyl)ethyl carbonate]

Base Information

Chemical Name:Adenosine, 3'-deoxy-N-[[2-(4-nitrophenyl)ethoxy]carbonyl]-, 5'-[6-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]hexanoate] 2'-[2-(4-nitrophenyl)ethyl carbonate]
CAS No.:193890-89-0
Molecular Formula:C49H48N8O14
Molecular Weight:972.965
Hs Code.:

Adenosine, 3'-deoxy-N-[[2-(4-nitrophenyl)ethoxy]carbonyl]-,
5'-[6-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]hexanoate]
2'-[2-(4-nitrophenyl)ethyl carbonate]

Synonyms:

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Chemical Property of Adenosine, 3'-deoxy-N-[[2-(4-nitrophenyl)ethoxy]carbonyl]-, 5'-[6-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]hexanoate] 2'-[2-(4-nitrophenyl)ethyl carbonate]

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Technology Process of Adenosine, 3'-deoxy-N-[[2-(4-nitrophenyl)ethoxy]carbonyl]-, 5'-[6-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]hexanoate] 2'-[2-(4-nitrophenyl)ethyl carbonate]

There total 3 articles about Adenosine, 3'-deoxy-N-[[2-(4-nitrophenyl)ethoxy]carbonyl]-, 5'-[6-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]hexanoate] 2'-[2-(4-nitrophenyl)ethyl carbonate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 88574-06-5
6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}hexanoic acid

: 97776-94-8
3'-deoxy-N⁶,2'-O-bis[2-(p-nitrophenyl)ethoxicarbonyl]adenosine

: 193890-89-0
6-(9H-Fluoren-9-ylmethoxycarbonylamino)-hexanoic acid (2S,4R,5R)-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; for 3.5h; Ambient temperature;
DOI:10.1002/hlca.19970800405

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 193890-89-0
6-(9H-Fluoren-9-ylmethoxycarbonylamino)-hexanoic acid (2S,4R,5R)-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / dimethylformamide; various solvent(s) / 1 h / Ambient temperature

2: 80 percent / EDC, DMAP / CH₂Cl₂ / 3.5 h / Ambient temperature

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19970800405

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 193890-89-0
6-(9H-Fluoren-9-ylmethoxycarbonylamino)-hexanoic acid (2S,4R,5R)-5-{6-[2-(4-nitro-phenyl)-ethoxycarbonylamino]-purin-9-yl}-4-[2-(4-nitro-phenyl)-ethoxycarbonyloxy]-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / dimethylformamide; various solvent(s) / 1 h / Ambient temperature

2: 80 percent / EDC, DMAP / CH₂Cl₂ / 3.5 h / Ambient temperature

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19970800405