Silane, [[4-(1,3-dioxolan-2-yl)phenyl]ethynyl]trimethyl-

Base Information Edit

Chemical Name:Silane, [[4-(1,3-dioxolan-2-yl)phenyl]ethynyl]trimethyl-
CAS No.:193903-54-7
Molecular Formula:C14H18O2Si
Molecular Weight:246.381
Hs Code.:
Mol file:193903-54-7.mol

Synonyms:

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Chemical Property of Silane, [[4-(1,3-dioxolan-2-yl)phenyl]ethynyl]trimethyl- Edit

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Technology Process of Silane, [[4-(1,3-dioxolan-2-yl)phenyl]ethynyl]trimethyl-

There total 3 articles about Silane, [[4-(1,3-dioxolan-2-yl)phenyl]ethynyl]trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 77123-57-0
4-[(trimethylsilyl)ethynyl]bezaldehyde

: 107-21-1
ethylene glycol

: 193903-54-7
4-trimethylsilylethynylbenzaldehyde ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Reflux; Inert atmosphere; Dean-Stark;
DOI:10.1016/j.jorganchem.2015.04.006

Reference yield: 93.0%

: 10602-01-4
p-bromobenzaldehyde 1,3-dioxolane

: 1066-54-2
trimethylsilylacetylene

: 193903-54-7
4-trimethylsilylethynylbenzaldehyde ethylene acetal

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In toluene; at 80 ℃; for 20h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c9cc06916j

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 193903-54-7
4-trimethylsilylethynylbenzaldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 12 h / 110 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide; triethylamine / toluene / 20 h / 80 °C / Inert atmosphere; Schlenk technique

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; triethylamine; In toluene;
DOI:10.1039/c9cc06916j