1,3-Dioxolane, 2-(4-ethynylphenyl)-

Base Information

Chemical Name:1,3-Dioxolane, 2-(4-ethynylphenyl)-
CAS No.:138853-09-5
Molecular Formula:C11H10O2
Molecular Weight:174.199
Hs Code.:
DSSTox Substance ID:DTXSID60478504
Wikidata:Q82311934
Mol file:138853-09-5.mol

Synonyms:1,3-Dioxolane, 2-(4-ethynylphenyl)-;138853-09-5;2-(4-ethynylphenyl)-1,3-dioxolane;SCHEMBL4012194;DTXSID60478504;IMBXCYXDOGCLNO-UHFFFAOYSA-N;10.14272/IMBXCYXDOGCLNO-UHFFFAOYSA-N.1;doi:10.14272/IMBXCYXDOGCLNO-UHFFFAOYSA-N.1

Suppliers and Price of 1,3-Dioxolane, 2-(4-ethynylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 1,3-Dioxolane, 2-(4-ethynylphenyl)-

Chemical Property:

Boiling Point:269.3±35.0 °C(Predicted)
PSA：18.46000
Density:1.15±0.1 g/cm3(Predicted)
LogP:1.71330
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:174.068079557
Heavy Atom Count:13
Complexity:201

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C#CC1=CC=C(C=C1)C2OCCO2

Technology Process of 1,3-Dioxolane, 2-(4-ethynylphenyl)-

There total 4 articles about 1,3-Dioxolane, 2-(4-ethynylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 193903-54-7
4-trimethylsilylethynylbenzaldehyde ethylene acetal

: 138853-09-5
4-ethynylbenzaldehyde ethylene acetal

Guidance literature:: With potassium carbonate; In methanol; for 12h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2015.04.006

Reference yield: 85.0%

: 63697-96-1
4-Ethynylbenzaldehyde

: 107-21-1
ethylene glycol

: 138853-09-5
4-ethynylbenzaldehyde ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 24h; Reflux; Dean-Stark;
DOI:10.1039/c4tc00399c

Reference yield: 49.0%

: 10602-01-4
p-bromobenzaldehyde 1,3-dioxolane

: 115-19-5
2-methyl-but-3-yn-2-ol

: 138853-09-5
4-ethynylbenzaldehyde ethylene acetal

Guidance literature:: p-bromobenzaldehyde 1,3-dioxolane; 2-methyl-but-3-yn-2-ol; With copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; for 20h; Heating;

With sodium hydride; In toluene; for 6h; Heating;
DOI:10.1039/b414302g