Technology Process of 2-[N-(diphenylphosphinothioylamino)-C-methylcarbonimidoyl]thiophene
There total 54 articles about 2-[N-(diphenylphosphinothioylamino)-C-methylcarbonimidoyl]thiophene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
cyclohexenone;
With
lithium diisopropyl amide;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.5h;
methyl iodide;
With
N,N,N,N,N,N-hexamethylphosphoric triamide;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 2h;
Further stages.;
DOI:10.1021/np049771x
- Guidance literature:
-
With
allyl methyl carbonate;
palladium diacetate; tributyltin methoxide; 1,2-bis-(diphenylphosphino)ethane;
In
acetonitrile;
for 10h;
Heating;
DOI:10.1016/S0040-4039(00)94161-3
- Guidance literature:
-
With
ozone;
In
dichloromethane;
at -78 ℃;
