ETHYL 2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]ACETATE

Base Information

• Chemical Name: ETHYL 2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]ACETATE
• CAS No.: 32418-24-9
• Molecular Formula: C6H9N3O2S2
• Molecular Weight: 219.288
• Hs Code.: 2934999090
• Mol file: 32418-24-9.mol

Synonyms:Aceticacid, [(5-amino-1,3,4-thiadiazol-2-yl)thio]-, ethyl ester (8CI,9CI);NSC 523973;

Chemical Property of ETHYL 2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]ACETATE

Chemical Property:

• Vapor Pressure: 6.7E-06mmHg at 25°C
• Refractive Index: 1.604
• Boiling Point: 377.5 °C at 760 mmHg
• Flash Point: 182.1 °C
• PSA: 131.64000
• Density: 1.43 g/cm³
• LogP: 1.35670

Purity/Quality:

99%, ^*data from raw suppliers

Ethyl [(5-amino-1,3,4-thiadiazol-2-yl)thio]acetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]ACETATE

There total 3 articles about ETHYL 2-[(5-AMINO-1,3,4-THIADIAZOL-2-YL)THIO]ACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

ethyl bromoacetate (105-36-2) + 2-Amino-5-mercapto-1,3,4-thiadiazole (2349-67-9) → ethyl 2-[(5-amino-1,3,4-thiadiazol-2-yl)thio]acetate (32418-24-9)

Guidance literature:

2-Amino-5-mercapto-1,3,4-thiadiazole; With potassium hydroxide; In ethanol; for 0.166667h;

ethyl bromoacetate; In ethanol; for 2h;

DOI:10.1002/cmdc.201300244

Reference yield:

chloroacetic acid ethyl ester (105-39-5) + 2-Amino-5-mercapto-1,3,4-thiadiazole (2349-67-9) → ethyl 2-[(5-amino-1,3,4-thiadiazol-2-yl)thio]acetate (32418-24-9)

Guidance literature:

With sodium hydroxide; In methanol; water; at 20 ℃; for 10h;

DOI:10.1016/j.cclet.2012.04.005

Reference yield:

→ ethyl 2-[(5-amino-1,3,4-thiadiazol-2-yl)thio]acetate (32418-24-9)

Guidance literature:

KOH, 2-Amino-5-mercaptan-1,3,4-thiadiazole, ethylchloroacetate;

upstream raw materials:

ethyl bromoacetate

2-Amino-5-mercapto-1,3,4-thiadiazole

chloroacetic acid ethyl ester

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