(2-Methylbenzyl)trimethylstannane

Base Information

Chemical Name:(2-Methylbenzyl)trimethylstannane
CAS No.:19962-44-8
Molecular Formula:C11H18Sn
Molecular Weight:268.96200
Hs Code.:
Mol file:19962-44-8.mol

Synonyms:Trimethyl-(2-methyl-benzyl)-stannane;Trimethyl-(o-tolyl-methyl)-zinn;(CH3)3SnCH2C6H4-o-CH3;

Suppliers and Price of (2-Methylbenzyl)trimethylstannane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (2-Methylbenzyl)trimethylstannane

Chemical Property:

Boiling Point:261.3±43.0 °C(Predicted)
PSA：0.00000
LogP:3.68130

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2-Methylbenzyl)trimethylstannane

There total 3 articles about (2-Methylbenzyl)trimethylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 612-12-4
o-Xylylene dichloride

: 1066-45-1
trimethyltin(IV)chloride

: 19962-44-8
α-(trimethylstannyl)-o-xylene

: 84457-41-0
α,alpha'.-bis(trimethylstannyl)-o-xylene

Guidance literature:: With magnesium; ethylene dibromide; In tetrahydrofuran; inert atmosphere, activation of Mg with ethylene bromide in THF, addn. of THF and a further portion of ethylene bromide, reflux, addn. of soln. of dichloro-o-xylene and soln. of (CH3)3SnCl to the boiling soln., reflux (6 h); saturated aq. NH4Cl, extn. (Et2O), washing of extracts (water), drying (Na2SO4), concn. (reduced pressure), distillation (92-95°C, 0.05 Torr);
DOI:10.1002/(SICI)1099-0682(199806)1998:6<761::AID-EJIC761>3.0.CO;2-1