Silane, trimethyl[[2-(phenylmethyl)-1-cyclohexen-1-yl]oxy]-

Base Information

Chemical Name:Silane, trimethyl[[2-(phenylmethyl)-1-cyclohexen-1-yl]oxy]-
CAS No.:200120-11-2
Molecular Formula:C16H24OSi
Molecular Weight:260.451
Hs Code.:
DSSTox Substance ID:DTXSID50470178
Nikkaji Number:J2.099.427D
Wikidata:Q82298177

Synonyms:Silane, trimethyl[[2-(phenylmethyl)-1-cyclohexen-1-yl]oxy]-;200120-11-2;SCHEMBL818172;DTXSID50470178

Suppliers and Price of Silane, trimethyl[[2-(phenylmethyl)-1-cyclohexen-1-yl]oxy]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, trimethyl[[2-(phenylmethyl)-1-cyclohexen-1-yl]oxy]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:260.159641919
Heavy Atom Count:18
Complexity:295

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)OC1=C(CCCC1)CC2=CC=CC=C2

Technology Process of Silane, trimethyl[[2-(phenylmethyl)-1-cyclohexen-1-yl]oxy]-

There total 6 articles about Silane, trimethyl[[2-(phenylmethyl)-1-cyclohexen-1-yl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 126269-41-8
(6-Benzyl-cyclohex-1-enyloxy)-trimethyl-silane

: 200120-11-2
(2-benzyl-cyclohex-1-enyloxy)-trimethyl-silane

Guidance literature:: With chloro{tris(o-tolyl)phosphine}gold(I); silver perchlorate; In 1,4-dioxane; at 100 ℃; for 2h;
DOI:10.3762/bjoc.7.76

Reference yield: 46.0%

: 75-77-4
chloro-trimethyl-silane

: 946-33-8
2-benzylcyclohexan-1-one

: 200120-11-2
(2-benzyl-cyclohex-1-enyloxy)-trimethyl-silane

Guidance literature:: 2-benzylcyclohexan-1-one; With lithium diisopropyl amide; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja8041542

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 200120-11-2
(2-benzyl-cyclohex-1-enyloxy)-trimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / 1 h / -78 °C

1.2: DMI

2.1: bromomagnesium diisopropylamide / tetrahydrofuran

2.2: Et₃N; HMPA / tetrahydrofuran

With bromomagnesium diisopropylamide; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ol0603007