2,3,9,10-Tetramethoxy-7-methyl-5,6-dihydrobenzo[c]acridine

Base Information

Chemical Name:2,3,9,10-Tetramethoxy-7-methyl-5,6-dihydrobenzo[c]acridine
CAS No.:204842-93-3
Molecular Formula:C22H23NO4
Molecular Weight:365.429
Hs Code.:
DSSTox Substance ID:DTXSID50599070
Wikidata:Q82494917

Synonyms:204842-93-3;2,3,9,10-Tetramethoxy-7-methyl-5,6-dihydrobenzo[c]acridine;SCHEMBL8501235;DTXSID50599070

Suppliers and Price of 2,3,9,10-Tetramethoxy-7-methyl-5,6-dihydrobenzo[c]acridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2,3,9,10-Tetramethoxy-7-methyl-5,6-dihydrobenzo[c]acridine

Chemical Property:

XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:365.16270821
Heavy Atom Count:27
Complexity:503

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2CCC3=CC(=C(C=C3C2=NC4=CC(=C(C=C14)OC)OC)OC)OC

Technology Process of 2,3,9,10-Tetramethoxy-7-methyl-5,6-dihydrobenzo[c]acridine

There total 2 articles about 2,3,9,10-Tetramethoxy-7-methyl-5,6-dihydrobenzo[c]acridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 4101-30-8
2-amino-4,5-dimethoxyacetophenone

: 13575-75-2
6,7-dimethoxy-1-oxo-1,2,3,4-tetrahydronaphthalene

: 204842-93-3
5,6-dihydro-2,3,9,10-tetramethoxy-7-methylbenz[c]acridine

Guidance literature:: With acetic acid; for 2h; Heating;
DOI:10.1016/j.bmc.2003.10.014

Reference yield:

: 4101-30-8
2-amino-4,5-dimethoxyacetophenone

: 204842-93-3
5,6-dihydro-2,3,9,10-tetramethoxy-7-methylbenz[c]acridine

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / diethyl ether; CH₂Cl₂ / 20 °C

2: 99 percent / 1 h / 140 °C

3: conc. NH₄OH / methanol / 20 °C / pH 10

With hydrogenchloride; ammonium hydroxide; In methanol; diethyl ether; dichloromethane; 1: Addition / 2: cyclocondensation / 3: Dehydrochlorination;
DOI:10.1016/S0968-0896(00)00048-1