4-(Diphenylphosphorothioyl)phenol

Base Information

Chemical Name:4-(Diphenylphosphorothioyl)phenol
CAS No.:20650-56-0
Molecular Formula:C18H15OPS
Molecular Weight:310.356
Hs Code.:
DSSTox Substance ID:DTXSID90393736
Nikkaji Number:J1.667.751E
ChEMBL ID:CHEMBL4649834

Synonyms:4-(diphenylphosphorothioyl)phenol;CHEMBL4649834;20650-56-0;4-(Diphenylphosphinothioyl)phenol;DTXSID90393736;BDBM50541266;STK372983;AKOS005447107

Suppliers and Price of 4-(Diphenylphosphorothioyl)phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 4-(Diphenylphosphorothioyl)phenol

Chemical Property:

PSA：62.13000
LogP:3.79860
XLogP3:5.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:310.05812327
Heavy Atom Count:21
Complexity:341

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=S)(C2=CC=CC=C2)C3=CC=C(C=C3)O

Technology Process of 4-(Diphenylphosphorothioyl)phenol

There total 7 articles about 4-(Diphenylphosphorothioyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 5068-21-3
4-(diphenylphosphanyl)phenol

: 20650-56-0
p-hydroxyphenyl(diphenyl)phosphine sulfide

Guidance literature:: With sulfur; In tetrahydrofuran;
DOI:10.1039/b104918f

Reference yield: 91.0%

: 14180-49-5
(4-methoxyphenyl)diphenylphosphine sulfide

: 20650-56-0
p-hydroxyphenyl(diphenyl)phosphine sulfide

Guidance literature:: With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 15h; Inert atmosphere;
DOI:10.1016/j.bmc.2020.115310

Reference yield:

: 795-44-8
4-(diphenylphosphoryl)benzonitrile

: 20650-56-0
p-hydroxyphenyl(diphenyl)phosphine sulfide

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorosilane / tetrahydrofuran; toluene / 2 h / 110 °C / Inert atmosphere

2: sulfur / tetrahydrofuran / 0.5 h / 120 °C / Microwave irradiation

3: boron tribromide / dichloromethane / 15 h / 0 - 20 °C / Inert atmosphere

With trichlorosilane; boron tribromide; sulfur; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.bmc.2020.115310