2-Hydroxy-4-[[2-hydroxy-4-methoxy-6-(3-oxopentyl)benzoyl]oxy]-6-pentylbenzoic acid

Base Information

Chemical Name:2-Hydroxy-4-[[2-hydroxy-4-methoxy-6-(3-oxopentyl)benzoyl]oxy]-6-pentylbenzoic acid
CAS No.:35578-70-2
Molecular Formula:C25H30 O8
Molecular Weight:0
Hs Code.:
Mol file:35578-70-2.mol

Synonyms:Miriquidicacid

Suppliers and Price of 2-Hydroxy-4-[[2-hydroxy-4-methoxy-6-(3-oxopentyl)benzoyl]oxy]-6-pentylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 2-Hydroxy-4-[[2-hydroxy-4-methoxy-6-(3-oxopentyl)benzoyl]oxy]-6-pentylbenzoic acid

Chemical Property:

PSA：130.36000
LogP:4.66820

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Hydroxy-4-[[2-hydroxy-4-methoxy-6-(3-oxopentyl)benzoyl]oxy]-6-pentylbenzoic acid

There total 10 articles about 2-Hydroxy-4-[[2-hydroxy-4-methoxy-6-(3-oxopentyl)benzoyl]oxy]-6-pentylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 105705-18-8
benzyl miriquidate

: 35578-70-2
miriquidic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 4h;

Reference yield:

: 35583-00-7
2-hydroxy-4-methoxy-6-(3-oxopentyl)benzoic acid

: 35578-70-2
miriquidic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 14 percent / trifluoroacetic anhydride / toluene / 2 h / Ambient temperature

2: 74 percent / H₂ / 10percent Pd/C / ethyl acetate / 4 h

With hydrogen; trifluoroacetic anhydride; palladium on activated charcoal; In ethyl acetate; toluene;

Reference yield:

: 105705-41-7
1-(2-bromo-3,5-dimethoxyphenyl)-3,3-diethoxypentane

: 35578-70-2
miriquidic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) PhLi / 1.) ether, RT, 24 h, 2.) ether, from -78 deg C to RT

2: 75 percent / BCl₃ / CH₂Cl₂ / 1.5 h / -78 - 20 °C

3: 14 percent / trifluoroacetic anhydride / toluene / 2 h / Ambient temperature

4: 74 percent / H₂ / 10percent Pd/C / ethyl acetate / 4 h

With hydrogen; boron trichloride; phenyllithium; trifluoroacetic anhydride; palladium on activated charcoal; In dichloromethane; ethyl acetate; toluene;