BZL-D-VAL-OME HCL

Base Information

• Chemical Name: BZL-D-VAL-OME HCL
• CAS No.: 210917-86-5
• Molecular Formula: C13H19NO2
• Molecular Weight: 221.299
• Hs Code.: 2922499990
• Mol file: 210917-86-5.mol

Synonyms:N-benzyl-D-valine methyl ester;

Chemical Property of BZL-D-VAL-OME HCL

Chemical Property:

• PSA: 38.33000
• LogP: 3.16670
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98% ^*data from raw suppliers

N-Benzyl-D-valine methyl ester hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of BZL-D-VAL-OME HCL

There total 1 articles about BZL-D-VAL-OME HCL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

D-Valine methyl ester hydrochloride (7146-15-8) + benzaldehyde (100-52-7) → N-benzyl-D-valine methyl ester (210917-86-5)

Guidance literature:

With sodium cyanoborohydride; In methanol; at 20 ℃;

DOI:10.1016/j.bmc.2003.09.015

Reference yield: 86.0%

N-methylsulfamoyl chloride (10438-96-7) + N-benzyl-D-valine methyl ester (210917-86-5) → methyl 2-(R)-[benzyl-(methylamino-sulfonyl)amino]-3-methylbutyrate (210917-30-9)

Guidance literature:

With hydrogenchloride; triethylamine;

Reference yield: 69.0%

allyl bromide (106-95-6) + N-benzyl-D-valine methyl ester (210917-86-5) → N-benzyl-N-allyl-D-valine methyl ester (684270-71-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 40 ℃;

DOI:10.1016/j.bmc.2003.09.015

upstream raw materials:

D-Valine methyl ester hydrochloride

benzaldehyde

Downstream raw materials:

N-benzyl-N-allyl-D-valine methyl ester

N-benzyl-N-(3-hydroxypropyl)-D-valine methyl ester

(2R,αR)-2-(4-methoxyphenyl)-α-(1-methylethyl)-2-oxo-1,3,2-oxazaphosphorinane-3-acetic acid

methyl (2R,αR)-2-(4-methoxyphenyl)-α-(1-methylethyl)-2-oxo-1,3,2-oxazaphosphorinane-3-acetate

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