Trimethyl[2-methylidene-4,4-bis(phenylsulfanyl)butyl]silane

Base Information

• Chemical Name: Trimethyl[2-methylidene-4,4-bis(phenylsulfanyl)butyl]silane
• CAS No.: 215182-46-0
• Molecular Formula: C20H26S2Si
• Molecular Weight: 358.644
• DSSTox Substance ID: DTXSID90578905
• Wikidata: Q82469250
• Mol file: 215182-46-0.mol

Synonyms:215182-46-0;DTXSID90578905;Trimethyl[2-methylidene-4,4-bis(phenylsulfanyl)butyl]silane

Chemical Property of Trimethyl[2-methylidene-4,4-bis(phenylsulfanyl)butyl]silane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 8
• Exact Mass: 358.12451971
• Heavy Atom Count: 23
• Complexity: 329

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)CC(=C)CC(SC1=CC=CC=C1)SC2=CC=CC=C2

Technology Process of Trimethyl[2-methylidene-4,4-bis(phenylsulfanyl)butyl]silane

There total 1 articles about Trimethyl[2-methylidene-4,4-bis(phenylsulfanyl)butyl]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

2-chloromethyl-3-trimethylsilyl-1-propene (18388-03-9) + bis(phenylthio)methane (3561-67-9) → Trimethyl-(2-methylene-4,4-bis-phenylsulfanyl-butyl)-silane (215182-46-0)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1016/S0040-4020(98)00745-5

Reference yield: 69.0%

12b-hydroxy-2,3-dimethoxy-5,12b-dihydro-6H-isoindolo[1,2-a]isoquinolin-8-one (188064-71-3) + Trimethyl-(2-methylene-4,4-bis-phenylsulfanyl-butyl)-silane (215182-46-0) → 2,3-dimethoxy-12b-(2-methyl-4,4-bis-phenylsulfanyl-but-2-enyl)-5,12b-dihydro-6H-isoindolo[1,2-a]isoquinolin-8-one

Guidance literature:

12b-hydroxy-2,3-dimethoxy-5,12b-dihydro-6H-isoindolo[1,2-a]isoquinolin-8-one; With titanium tetrachloride; In dichloromethane; at -78 ℃; for 1h;

Trimethyl-(2-methylene-4,4-bis-phenylsulfanyl-butyl)-silane; In dichloromethane; at -78 ℃; Further stages.;

DOI:10.1016/j.tetlet.2003.11.122

Reference yield:

Trimethyl-(2-methylene-4,4-bis-phenylsulfanyl-butyl)-silane (215182-46-0) → Trimethyl-(2-methylene-4-phenylsulfanyl-butyl)-silane (125564-77-4)

Guidance literature:

With N,N-dimethyl-1-naphthalenamine; lithium; In tetrahydrofuran; at -45 ℃; for 1.5h;

DOI:10.1016/S0040-4020(98)00745-5

upstream raw materials:

2-chloromethyl-3-trimethylsilyl-1-propene

bis(phenylthio)methane

Downstream raw materials:

Trimethyl-(2-methylene-4-phenylsulfanyl-butyl)-silane

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