Germane, iodotriphenyl-

Base Information

Chemical Name:Germane, iodotriphenyl-
CAS No.:2181-43-3
Molecular Formula:C18H15GeI
Molecular Weight:430.812
Hs Code.:
DSSTox Substance ID:DTXSID00464249
Nikkaji Number:J1.728.880F

Synonyms:Germane, iodotriphenyl-;2181-43-3;triphenylgermanium iodide;SCHEMBL10781303;DTXSID00464249

Suppliers and Price of Germane, iodotriphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Germane, iodotriphenyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:431.94303
Heavy Atom Count:20
Complexity:240

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Ge](C2=CC=CC=C2)(C3=CC=CC=C3)I

Technology Process of Germane, iodotriphenyl-

There total 9 articles about Germane, iodotriphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 556-56-9
allyl iodid

: 2816-43-5
triphenylgermane

: 2181-43-3
triphenylgermanium iodide

Guidance literature:: With benzene; palladium dichloride; In neat (no solvent); ligand, Ge-compound and PdCl2 were stirred at at room temp., benzene wasadded after 6 h, stirred for 12 h under inert atm.; elem. anal.;
DOI:10.1016/S0022-328X(02)02147-2

Reference yield: 61.0%

: 3005-32-1
triphenylgermanium bromide

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 2181-43-3
triphenylgermanium iodide

Guidance literature:: In acetone; byproducts: NaBr; NaI added to acetone with stirring, triphenylgermanium bromide dissolvedin acetone and added to the NaI acetone mixture, refluxed overnight; cold hexane added, filtered, solvent evaporated, recrystallized from diethyl ether, elem. anal.;
DOI:10.1039/b105457k

Reference yield:

: 2816-39-9
hexaphenyldigermane

: 2181-43-3
triphenylgermanium iodide

Guidance literature:: Multi-step reaction with 6 steps

1: ammonia

2: diethyl ether

3: further solvent(s)

4: ammonia

5: not given

6: water

In diethyl ether; ammonia; water;