2-Benzylbuta-2,3-dienol

Base Information

Chemical Name:2-Benzylbuta-2,3-dienol
CAS No.:2219-53-6
Molecular Formula:C11H12O
Molecular Weight:160.216
Hs Code.:
DSSTox Substance ID:DTXSID501307355
Nikkaji Number:J1.797.435A

Synonyms:2-benzylbuta-2,3-dienol;2219-53-6;beta-Ethenylidenebenzenepropanol;SCHEMBL12003573;GZLATWWTNLJYDL-UHFFFAOYSA-N;DTXSID501307355

Suppliers and Price of 2-Benzylbuta-2,3-dienol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Benzylbuta-2,3-dienol

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:160.088815002
Heavy Atom Count:12
Complexity:171

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=C=C(CC1=CC=CC=C1)CO

Technology Process of 2-Benzylbuta-2,3-dienol

There total 6 articles about 2-Benzylbuta-2,3-dienol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 433733-19-8
2-benzyl-buta-2,3-dienoic acid ethyl ester

: 2219-53-6
2-benzylbuta-2,3-dien-1-ol

Guidance literature:: With diisobutylaluminium hydride; In toluene; at -78 ℃; for 4h;
DOI:10.1021/jo0108616

Reference yield: 48.0%

: C₁₂H₁₀O₃

: 2219-53-6
2-benzylbuta-2,3-dien-1-ol

Guidance literature:: With copper(l) cyanide; isopropyl alcohol; 1,3-dicyclohexyl-1H-imidazol-3-ium chloride; sodium t-butanolate; 2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-5,5-dimethyl-1,3,2-dioxaborinane; In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere; Glovebox;
DOI:10.1002/anie.202014310

Reference yield:

: 26599-08-6
ethyl 3-phenyl-2-(triphenylphosphoranylidene)propanoate

: 2219-53-6
2-benzylbuta-2,3-dien-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / CH₂Cl₂

2: 62 percent / DIBAL-H / toluene / 3.5 h / -78 °C

With diisobutylaluminium hydride; triethylamine; In dichloromethane; toluene;
DOI:10.1021/jo0163997