(4-Iodo-2-methylphenyl)hydrazine

Base Information

• Chemical Name: (4-Iodo-2-methylphenyl)hydrazine
• CAS No.: 227015-67-0
• Molecular Formula: C7H9IN2
• Molecular Weight: 248.066
• DSSTox Substance ID: DTXSID90591659
• Wikidata: Q82485490
• Mol file: 227015-67-0.mol

Synonyms:(4-Iodo-2-methylphenyl)hydrazine;227015-67-0;SCHEMBL6561965;4-hydrazino-3-methyliodobenzene;DTXSID90591659;BCTUYVACDFZUFZ-UHFFFAOYSA-N;DB-179280;EN300-6494388

Chemical Property of (4-Iodo-2-methylphenyl)hydrazine

Chemical Property:

• PSA: 38.05000
• LogP: 2.65850
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 247.98105
• Heavy Atom Count: 10
• Complexity: 108

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1)I)NN

Technology Process of (4-Iodo-2-methylphenyl)hydrazine

There total 1 articles about (4-Iodo-2-methylphenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-methylphenyl)acetamide (120-66-1) → (4-iodo-2-methyl-phenyl)-hydrazine (227015-67-0)

Guidance literature:

Multi-step reaction with 2 steps

1: iodine chloride / Verseifung des entstandenen 5-Jod-2-acetamino-toluols

2: Diazotization_.man behandelt das entstandene Diazoniumsalz mit Kaliumsulfit und reduziert das Produkt mit Zinnchloruer und Salzsaeure

With Iodine monochloride;

Reference yield: 96.0%

4-methoxyphenylboronic acid (5720-07-0) + (4-iodo-2-methyl-phenyl)-hydrazine (227015-67-0) → 4'-methoxy-3-methylbiphenyl (17171-17-4)

Guidance literature:

(4-iodo-2-methyl-phenyl)-hydrazine; With polystyrene-NHCO(CH₂)4COOH; benzotriazol-1-ol; diisopropyl-carbodiimide; In dichloromethane;

4-methoxyphenylboronic acid; With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; In N,N-dimethyl-formamide; at 80 ℃; for 24h;

With propylamine; copper diacetate; at 20 ℃; for 2h;

DOI:10.1002/(SICI)1521-3773(19990419)38:8<1073::AID-ANIE1073>3.0.CO;2-Y

Reference yield: 83.0%

(E)-3-dimethylamino-2-[5-(morpholine-4-carbonyl)-1-(2-trimethylsilanyl-ethoxymethyl)-1H-indole-2-carbonyl]-acrylonitrile + (4-iodo-2-methyl-phenyl)-hydrazine (227015-67-0) → [5-amino-1-(4-iodo-2-methyl-phenyl)-1H-pyrazol-4-yl]-[5-(morpholine-4-carbonyl)-1-(2-trimethylsilanyl-ethoxymethyl)-1H-indol-2-yl]-methanone

Guidance literature:

In ethanol; at 78 ℃; for 16h;

upstream raw materials:

N-(2-methylphenyl)acetamide

Downstream raw materials:

4'-methoxy-3-methylbiphenyl

4-{3-[4-(3-(2-ethoxycarbonyl-ethyl)-5-phenyl-pyrazol-1-yl)-3-methyl-phenyl]-propargylamino}benzamidine

4-{3-[4-(3-(2-hydroxycarbonyl-ethyl)-5-phenyl-pyrazol-1-yl)-3-methyl-phenyl]-propargylamino}benzamidine

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