2,16-DIOXATETRACYCLO[11.2.1.0(3,12).0(6,11)]HEXADECA-3(12),4,6(11),7,9-PENTAENE

Base Information

• Chemical Name: 2,16-DIOXATETRACYCLO[11.2.1.0(3,12).0(6,11)]HEXADECA-3(12),4,6(11),7,9-PENTAENE
• CAS No.: 22794-75-8
• Molecular Formula: C₁₄H₁₂O₂
• Molecular Weight: 212.248
• Mol file: 22794-75-8.mol

Synonyms:1,2,3,4-tetrahydro-1,4-epioxido-naphtho[2,1-b]oxepine;

Chemical Property of 2,16-DIOXATETRACYCLO[11.2.1.0(3,12).0(6,11)]HEXADECA-3(12),4,6(11),7,9-PENTAENE

Chemical Property:

• Melting Point: 91 - 93 °C
• PSA: 18.46000
• LogP: 3.40980

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2,16-DIOXATETRACYCLO[11.2.1.0(3,12).0(6,11)]HEXADECA-3(12),4,6(11),7,9-PENTAENE

There total 2 articles about 2,16-DIOXATETRACYCLO[11.2.1.0(3,12).0(6,11)]HEXADECA-3(12),4,6(11),7,9-PENTAENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis,trans-2,5-dimethoxytetrahydrofuran (696-59-3) + β-naphthol (135-19-3) → 1,4-epoxy-1,2,3,4-tetrahydronaphth<2,1-b>oxepin (22794-75-8)

Guidance literature:

DOI:10.1016/S0040-4039(97)00404-8

Reference yield:

→ 1,4-epoxy-1,2,3,4-tetrahydronaphth<2,1-b>oxepin (22794-75-8)

Guidance literature:

Verb.1, Verb.3;

DOI:10.1021/jo00828a072

Reference yield:

1,4-epoxy-1,2,3,4-tetrahydronaphth<2,1-b>oxepin (22794-75-8) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → (2,4-dinitro-phenyl)-(1,2,3,4-tetrahydro-1,4-epiazano-naphtho[2,1-b]oxepin-12-yl)-amine (22794-77-0)

Guidance literature:

With sulfuric acid; In ethanol; Ambient temperature;

DOI:10.1021/jo00828a072

upstream raw materials:

cis,trans-2,5-dimethoxytetrahydrofuran

β-naphthol

Downstream raw materials:

(2,4-dinitro-phenyl)-(1,2,3,4-tetrahydro-1,4-epiazano-naphtho[2,1-b]oxepin-12-yl)-amine

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