2-Methyl-3-oxo-2-phenylbutanenitrile

Base Information

Chemical Name:2-Methyl-3-oxo-2-phenylbutanenitrile
CAS No.:22872-40-8
Molecular Formula:C11H11NO
Molecular Weight:173.21100
Hs Code.:
Mol file:22872-40-8.mol

Synonyms:2-methyl-2-phenyl-acetoacetonitrile;2-Methyl-3-oxo-2-phenylbutanenitrile;2-Methyl-2-phenyl-acetoacetonitril;

Suppliers and Price of 2-Methyl-3-oxo-2-phenylbutanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Methyl-3-oxo-2-phenylbutanenitrile 95+%
1g
$ 698.00

Alichem
2-Methyl-3-oxo-2-phenylbutanenitrile
1g
$ 607.76

Total 4 raw suppliers

Chemical Property of 2-Methyl-3-oxo-2-phenylbutanenitrile

Chemical Property:

PSA：40.86000
LogP:2.05688

Purity/Quality:

99% ^*data from raw suppliers

2-Methyl-3-oxo-2-phenylbutanenitrile 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Methyl-3-oxo-2-phenylbutanenitrile

There total 6 articles about 2-Methyl-3-oxo-2-phenylbutanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 75-36-5
acetyl chloride

: 164594-13-2
Phenyl[2-(trimethylsilyl)phenyl]iodonium trifluoromethanesulfonate

: 107-12-0
propiononitrile

: 22872-40-8
2-methyl-3-oxo-2-phenyl-butyronitrile

Guidance literature:: propiononitrile; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.25h;

Phenyl[2-(trimethylsilyl)phenyl]iodonium trifluoromethanesulfonate; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 0.916667h;

acetyl chloride; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1080/00397910600943402

Reference yield:

: 77-78-1
dimethyl sulfate

: 4468-48-8
1-phenyl-1-cyanopropan-2-one

: 22872-40-8
2-methyl-3-oxo-2-phenyl-butyronitrile

: 73591-13-6
3-methoxy-2-phenyl-2-butenenitrile

Guidance literature:: With sodium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 20 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;